光纤光栅弹簧管压力传感器的压力和温度特性

本文利用弹簧管对于压力的机械放大作用,将弹簧管与光纤光栅悬臂梁调谐技术相结合,研制了一种新颖的光纤光栅弹簧管压力传感器,大大提高了光纤布喇格光栅对压力测量的灵敏度,压力灵敏度系数可达-1.79×10^-4/MPa,比裸光栅提高了两个数量级,在0～12MPa的压力范围内,光纤布喇格光栅中心反射波长的改变与压力成良好的线性关系.同时由于悬臂梁热膨胀效应的影响,光纤光栅的温度灵敏度提高为裸光栅的7倍.     

基于偶联剂技术的光纤光栅压力传感实验研究

报道了利用偶联技术封装光纤光栅压力传感器的新方案.通过采用特殊聚合物材料将光纤光栅封装于金属管中，并采用偶联材料分别与聚合物和光纤以化学键偶联的工艺，解决了由于有机弹性体聚合物的弹性模量（1.2×105 N/m2）与光纤光栅的弹性模量(7×1010 N/m2)相差很大，在压强较大时易导致光纤光栅与聚合物材料之间的撕裂滑脱问题，改善了光纤光栅压力响应特性.封装后的光纤光栅压力的线性测量范围为0.04 MPa~0.6 MPa，压力响应灵敏度为－4.48 nm/MPa，与裸光栅压力响应灵敏度－0.003063 nm/MPa相比，增敏了1463倍.利用实验中所使用光谱仪0.05 nm的分辨率，压强测量准确度为±0.01 MPa，线性度为0.9978.     

双波长高灵敏度Bragg光纤光栅压力传感器

裸光纤光栅压力灵敏度只有 -2. 05×10-6 /MPa,这样并不能将其用于低压力范围内的测量 本文改进了封装结构,利用金属管结构对光纤光栅部分封装,制作成双波长高灵敏度光纤光栅压力传感器 其压力灵敏度在 0~0. 44MPa的范围内可达-2. 44×10-3 /MPa,是裸光栅的 1200倍,大大提高了光纤光栅压力传感的灵敏度 采用自行研制的Bragg光纤光栅,其反射波长为 1558. 00 nm,峰值反射率为 99% 封装后的Bragg光纤光栅位于铜管的轴心,将其一部分 (约光纤光栅的二分之一 )封装到长 25mm,外径 10mm厚为 0. 8mm的铜管内 室温为 18℃时将封装好的光…     

聚合物封装的高灵敏度光纤Bragg光栅温度传感器

将光纤光栅封装于一种有机聚合物基底中,制成温敏元件,测量了20～100℃不同温度下光纤光栅的反射谱.由于基底材料的带动作用,封装后的光纤光栅温度灵敏度为83.07×10-6/℃,是相应裸光纤光栅的12.3倍.     

高灵敏度光纤光栅压力传感器及其压力传感特性的研究

采用增敏罐封装的方法 ,设计并研究了一种新型高灵敏度的光纤光栅压力传感器 ,其压力灵敏系数可高达- 3.41× 10 - 3 MPa- 1 (相应于灵敏度 - 5 .2 77nm MPa) ,压力灵敏系数较裸光纤提高了 172 2倍 ,且线性度良好 ,可应用于低压情况下物理量的传感测量     

基于沉淀工艺制作四脚氧化锌纳米材料场致发射阴极的研究

采用沉淀法制备四脚氧化锌纳米材料场致发射阴极，将阴极和荧光屏封装起来抽真空并对屏施加电压，测试阴极的发射电流和荧光屏的发光亮度.利用沉淀法制备出面积为(13×15) cm²的阴极，测试结果表明，硅酸钾体积百分比在50×10^-3—83×10^-3范围，硝酸钡浓度在50×10^-4—77×10^-4 M范围，四脚氧化锌的浓度在82×10^-4—12×10^{-3相似文献}   

光纤Bragg光栅热敏力敏效应研究及应用探讨

本文报道了光纤Bragg光栅热敏力敏效应的实验研究结果,测量所得的光纤Bragg光栅温度系数和应力系数分别为6.84×10^-6/℃和7.27×10^-6/gf,与理论值6.85×10^-6/℃和7.32×10^-6/gf符合得很好.在20～180℃和0～50gf的温度应力测量范围内,光纤Bragg光栅透射谱中心波长移动量同温度应力具有良好的线性关系.基于光纤Bragg光栅的热敏力敏效应,本文还讨论了光纤Bragg光栅温度应变传感器实用化时必须首先考虑的一些关键问题.     

流体静压力对InSb输运性质的影响

在室温和流体静压力达12500公斤/厘米²下,测量了不同掺杂浓度的n型(5×10¹³—2.3×10¹⁸厘米^-3和p型(2.6×10¹⁴—6.0×10¹⁷厘米^-3)InSb的霍耳系数和电导率。分析结果发现,霍耳系数公式中散射因子随压力而减小,禁带宽的压力系数不是常数;得出禁带宽、载流子浓度、电子和空穴迁移率与压力的关系,并对压力下的载流子散射机构作了初步讨论。     

聚合物封装的高灵敏度光纤光栅温度传感器及其低温特性

介绍了一种新型的光纤光栅温度传感器。这种光纤光栅温度传感器使用了特殊的工艺将光纤布拉格光栅封装于一种热膨胀系数较大的有机聚合物基底中 ,使得传感器的温度灵敏性比裸光纤光栅提高了 12 .3倍 ,其温度灵敏度系数KT 达到 82 .6 9× 10 -6/℃。在 - 80～ 0℃的低温度范围内 ,对这种新型光纤光栅温度传感器的反射谱进行了测量。研究了这种新型光纤光栅温度传感器的低温特性 ,并与裸光纤光栅和铝基封装的光纤光栅进行了比较 ,结果表明这种新型的光纤光栅温度传感器具有很好的低温响应特性。     

克里奇中间体CH2OO与CF3CF=CF2反应的动力学研究

本文使用OH激光诱导荧光方法研究了结构最简单的克里奇中间体CH₂OO和CF₃CF=CF₂的反应动力学. 在压强为10 Torr条件下，测量了温度在283，298，308和318 K的反应速率常数，分别为(1.45±0.14)×10^-13，(1.18±0.11)×10^-13，(1.11±0.08)×10^-13和(1.04±0.08)×10^-13 cm³·molecule^-1·s^-1. 根据阿伦尼乌斯方程，获得该反应的活化能为(-1.66±0.21) kcal/mol. 在6.3∽70 torr压力范围内，未观察到该反应的速率常数存在压力相关.     

耐高压光纤Bragg光栅压力传感技术研究

分析了聚合物封装光纤光栅的压力响应特性,通过采用特殊聚合物材料将光纤光栅封装于金属套管中,并通过在金属套管预涂覆一层软弹性材料,以消除封装过程中由于聚合物固化收缩以及聚合物与套管壁粘接与摩擦产生的光纤光栅啁啾化,改善了光纤光栅压力响应特性.封装后的光纤光栅压力响应灵敏度为0.036 nm/MP,具有良好的线性,压力测量范围可达40 MP以上.     

Dissociation of the light-harvesting membrane protein complex I from Rhodobacter sphaeroides under high hydrostatic pressure

The light-harvesting complex 1 (LH1) from Rhodobacter sphaeroides is an excellent model system for investigating the stability of oligomeric membrane proteins under high hydrostatic pressure. The currently investigated LH1 forms a 16-meric ring structure of B825 subunits. B825 is a heterodimer of transmembrane α- and β-polypeptide chains, which non-covalently binds two bacteriochlorophyll a molecules. These pigment molecules were used as intrinsic spectroscopic sensors to follow the dissociation reaction. Our results demonstrate that the LH1 dissociates into B825 subunits through an intermediary tetrameric unit B845. The dissociation mechanism depends on pressure. At ～200–500?MPa the dissociation corresponds to a pseudo-first-order reaction, characterised by the apparent reaction rate at atmospheric pressure k₀?=?3·10^?5?s^?1, activation volume ΔV^??=??4?mL/mol, and free energy of activation ΔG^??=?26?kJ/mol. Below 200?MPa and above 500?MPa, the reaction is more complex, including further dissociation of B825 into monomers B777.     

High Temperature Sensitive Fiber Bragg Grating with Polymer Jacket

It is demonstrated the high thermal sensitivity of fiber Bragg grating with polymer jacket. Twenty-three times enhanced sensitivity and over 41nm Bragg wavelength-tuning range have been obtained when the fiber grating is packaged with a special kind of polymer. This is the largest thermal sensitivity and largest temperature-tuned range ever demonstrated to our knowledge.     

High Temperature Sensitive Fiber Bragg Grating with Polymer Jacket

1IntreduCionFtherBragggratingsareattractingconsiderableinterestf0rtheirextensiveapp1icatboin0PticalteIecommunicatiOnandfibersensor8yStems['~'J.A1argetuningrange0fBraggwavelengthis0ftenrequlredinmanyaPplicati0nsintuningdevicesf0rlasers0rfilterselementSf0rWDMsyStems.Inthecase0ffibergratingtemperaturesensors,alargethermalsensitivityisalsodesired.Theorigina1temPeraturesensitivity0fthefibergratingSisonlyabout0.01nrn/tnear155Onmbecauseofthesmallthermo-oPticandthermalexPansi0ncoefficientoffus…     

光纤光栅边孔封装技术

提出了一种新型的光纤光栅压力增敏封装技术——边孔封装技术,它通过改变封装体的几何结构实现了高倍数的压力增敏效果,较大程度减小了压力增敏倍数对聚合物材料参量的依赖性。采用有限元理论建立了边孔封装结构的压力传感模型,分析了封装体几何结构变化对封装后压力灵敏度的影响。采用聚合物材料进行了封装制作实验,测量结果表明封装后光纤光栅的压力灵敏度为5251 pm/MPa,是封装前压力灵敏度的1750倍,并将交叉敏感问题改善了近三个数量级,可满足高精度水下压力测量的应用要求。     

用光纤光栅的啁啾效应实现温度不敏感的弯曲传感

本文首次将光纤布喇格光栅在梯度分布的应变作用下产生的啁啾效应应用于弯曲传感,提出了一种新颖的光纤光栅弯曲传感方法.由于传感量为光纤光栅的带宽,传感测量完全避开了温度的交叉敏感效应,实验测量得到了很好的线性响应.基于光谱分析仪0.1nm的光谱分辨率,实验的曲率分辨率为0.036m^-1,测量范围可达4m^-1.     

A true fiber optic refractometer

The best instrument to measure the refractive index of liquids is the Abbe refractometer which can only provide accuracies of the order of 10⁻⁵ at visible wavelengths and 10⁻⁴ in the near infrared. Here we present a technique by which the exact wavelength positions in the near infrared frequency comb of a tilted grating inscribed in the core of an optical fiber can be used to measure the absolute value of the refractive index of a liquid in which the fiber is inserted, with an accuracy of ±5×10⁻⁵. This is in contrast to typical fiber optic‐based “refractometry” where only refractive index variations can be measured accurately, hence the appellation of “true” fiber optic refractometer here. In addition to the increased accuracy, the fiber refractometer proposed here offers the additional advantages associated with in situ measurements. The performance of this refractometer is demonstrated by measurements in water from room temperature down to near freezing at wavelengths in the 1550 nm window.

     

The permittivities of PVDF/PMMA blends at hydrostatic pressure

The complex permittivities of poly(vinylidene fluoride)/poly(methyl methacrylate) (PVDF/PMMA) blends have been measured under variation of temperature T(20°-60°C), frequency v(5 Hz-300 kHz), and hydrostatic pressure p (0-260 MPa). The values can be represented by a master curve with the shift factors △p/△ log (v/Hz) = ?140 MPa at room temperature and △ (1 /T) /△ log (v/Hz) = ?2. 10^?4 K^?1 at atmospheric pressure. The dependence of the activation energy △E _A on pressure p is then given by △E _A=(100 + 0.02 MPa^?1 p) kJ/mol. Furthermore, the results indicate that the β-relaxation of PVDF is due to motions in the crystal-amorphous interphase. The interactions between the two polymers, which are miscible at all compositions, disturb the correlations between the PVDF monomer units at that location as well as the mobility of the PMMA side group.