Measurement of the spectral dispersion curves of low birefringence polymer fibres

A method is suggested to overcome the difficulties of measuring the spectral dispersion of low birefringence fibres, that produce small optical path difference, δ<3λ, where δ is the optical path difference and λ is the wavelength of light used. This method depends on variable wavelength interferometry (VAWI). The suggested method is used to measure the spectral dispersion of birefringence of polypropylene fibre with a draw ratio 4 (low birefringence fibre). This method is also used to measure the spectral dispersion of birefringence of a polyester staple from ICI (high birefringence fibre). Also, the conventional VAWI method is used to measure the spectral dispersion of this fibre to confirm the results obtained by the suggested method. Microinterferograms are given for illustration.     

Comparative experimental study on absolute measurement of spherical surface with two-sphere method

The two-sphere method with multiple confocal measurements and a “cat's-eye” measurement is used widely in high accuracy interferometry, which can obtain the absolute surface data of the tested spherical surface. We provide a comparative experimental study on absolute testing procedures for spherical surface with two-sphere method, which include the classical Jensen method with three position measurements, the Zygo method with five position measurements and a variant of the Jensen method. The variant of the Jensen method can combine the multiple “three-position” measurements based on the fiducial method and averaging method. The repeatability of the involved absolute measurement methods is also studied by the five set experiments, and the corresponding Zernike fitting coefficients are compared in detail. The experimental results are meaningful for implementation of two-sphere method with higher repeatability in practice.     

Rare transition event with self-consistent theory of large-amplitude collective motion

A numerical simulation method, based on Dang et al.’s self-consistent theory of large-amplitude collective motion, for rare transition events is presented. The method provides a one-dimensional pathway without knowledge of the final configuration, which includes a dynamical effect caused by not only a potential but also kinetic term. Although it is difficult to apply the molecular dynamics simulation to a narrow-gate potential, the method presented is applicable to the case. A toy model with a high-energy barrier and/or the narrow gate shows that while the Dang et al. treatment is unstable for a changing of model parameters, our method stable for it.     

Mass-spectrometric monitoring of the stress reaction during anesthesia

Clinical testing data for a mass-spectrometric method of estimating the patient’s stress reaction to an injury done during anesthesia are presented. The essence of the method is monitoring the respiratory coefficient, which is defined as ratio N of the expiratory mass concentration of CO₂ to the inspiratory mass concentration of O₂ at each breathing cycle. For on-line monitoring of N, an electron ionization mass spectrometer connected to the breathing circuit of an inhalational anesthesia machine is used. Estimates of the anesthesia adequacy obtained with this method are compared with those obtained with the method that analyzes induced acoustic encephalographic potentials. It is shown that the method suggested is more sensitive to the level of the patient’s stress reaction during anesthesia than the induced potential method.     

Determination of parameters of phase element under conditions of multiray interference

The method of measuring the phase shift Γ and the relative amplitude transmission coefficient F of a phase element is developed and experimentally tested. The conditions minimizing an experimental error of measuring Γ and F are determined. The accuracy of the proposed method is shown to be comparable to that of the currently used one; however, the proposed method is simpler and allows automation.     

Multi-dimensional mixed quantum–classical description of the laser-induced desorption of molecules

A mixed quantum–classical method for the simulation of laser-induced desorption processes at surfaces is implemented. In this method, the nuclear motion is described classically, while the electrons are treated quantum mechanically. The feedback between nuclei and electrons is taken into account self-consistently. The computational efficiency of this method allows a more realistic multi-dimensional treatment of desorption processes. We apply this method to the laser-induced desorption of NO from NiO(100) using a two-state two-dimensional potential energy surface derived from ab initio quantum chemical calculations; we extend this potential energy surface to seven dimensions employing a physically reasonable model potential. By comparing our method to jumping wave-packet calculations on exactly the same potential energy surface we verify the validity of our method. We focus on the velocity, rotational, and vibrational distributions of the desorbing NO molecules. Furthermore, we model the energy transfer to the substrate by a surface oscillator. Including recoil processes in the simulation has a decisive influence on the desorption dynamics, as far as the velocity and rotational distribution is concerned. In particular, the bimodality in the velocity distribution observed in low dimensions and in the experiment disappears in a high-dimensional treatment. PACS  68.43.Tj; 68.43.Rs; 82.20.Gk; 82.20.Wt     

Identification of inherent noise components of semiconductor devices on an example of optocouplers

In the paper, a method of estimation of parameters of Gaussian and non-Gaussian components in the noise signal of semiconductor devices in a frequency domain is proposed. The method is based on composing estimators of two spectra, corresponding to 1/f^α noise (Gaussian component) and two-level RTS noise (non-Gaussian component). The proposed method can be applied for precise evaluation of the corner RTS frequency fRTS in the noise spectrum.     

The light transmission method of automated track scanning

An empirical method of automated track scanning is described. This new method is based on the measurement of light transmission (LT) through solid state track recorders (SSTR). Fission fragment tracks in mica SSTR are used to demonstrate the utility of this method. Data analysis reveals that the LT method is equivalent to a point sampling method at the approximately 2% (1σ) uncertainty level of the calibration data. The total (1σ) uncertainty of the LT method decreases with increasing fission density from approximately 5% at a fission density of 4.0E + 06 fissions/cm² down to approximately 2.5% at a fission density of 1.2E + 07 fissions/cm². The current stage of development permits only a qualitative comparison of the LT and point sampling methods. Recommendations to refine the LT method are advanced with emphasis on processing procedures for mica SSTR.     

Laser pulse transient method for measuring the normal spectral emissivity of samples with arbitrary surface quality

A laser pulse transient method for measuring normal spectral emissivity is described. In this method, a laser pulse (λ=1064 nm) irradiates the top surface of a flat specimen. A two-dimensional temperature response of the bottom surface is measured with a calibrated thermographic camera. By solving an axisymmetric boundary value heat conduction problem, the normal spectral emissivity at 1064 nm is determined by using an iterative nonlinear least-squares estimation procedure. The method can be applied to arbitrary sample surface quality. The method is tested on a nickel specimen and used to determine the normal spectral emissivity of AISI 304 stainless steel. The expanded combined uncertainty of the method has been estimated to be 18%.     

Method of systems of equations of P-adic coverages for fractal analysis of events

Self-similarity in high-energy multiparticle production processes is discussed. A parton shower and hadronization are assumed to give rise to a set of particle with a fractal structure. It is noted that the box counting (BC) and P-adic coverage (PaC) methods determine the fractal dimension with permissible 1/k ranges. A new method of systems of equations of P-adic coverages (SePaC) is proposed that extends the PaC method to fractals with permissible m/k ranges. The SePaC method is shown to determine the fractal dimension of a shower with a prescribed accuracy, the number of fractal levels, the type of the cascade (random or regular), and its structure.     

Comparison of eight unwrapping algorithms applied to Fourier-transform profilometry

Phase unwrapping is a task common to many applications like interferometry imaging, medical magnetic resonance imaging, solid-state physics, etc. Fourier transform profilometry (FTP) values the height distribution of object, elaborating the interference between a plane reference grating and a deformed object grating. Since the height information is extracted from the phase of a complex function, the phase unwrapping is a critical step of the process. Several unwrapping algorithms are proposed in literature, but applied to measurement technologies different from FTP. The purpose of this paper is to define the performances of eight different unwrapping algorithms applied to FTP optical scan method and to define the best one. The algorithms chosen are: Goldstein's algorithm, quality guided path following method, Mask cut method, Flynn's method, multi-grid method, weighted multi-grid method, preconditioned conjugate gradient method and minimum L_p-norm method. The methods were tested on real images acquired by a FTP scanner developed and calibrated for these experiments. The objects used vary from simple geometries, like planes and cylinders, to complex shapes of common use objects. Algorithms were qualified considering the phase unwrapping errors, execution time and accuracy of the shape of objects obtained from the scan method in comparison with real ones. The results show that quality guided algorithm best fits in FTP application.     

构造Birkhoff表示的广义Hojman方法

研究第一积分、Hojman方法及Birkhoff方程之间的内在联系. Hojman方法构造的Birkhoff函数(组)满足的一个特定关系, 对此关系加以分析得到更为一般的广义Hojman方法. 再将此关系与Birkhoff方程相结合, 导出Birkhoff系统Hojman意义下的循环积分. 举例说明结论的应用. 关键词： Birkhoff系统 Hojman方法 广义Hojman方法 循环积分     

Application of Atomic Fluorescence Spectrometry to the Determination of Sulfide Ion in Sewage Waters

Atomic fluorescence spectrometry and direct flame photometry are evaluated as alternative methods for the determination of inorganic sulfide in municipal sewage. The sulfide is volatilized as H₂S from the sewage influent or effluent sample, which has been stabilized by a 0.05 M sodium ascorbate buffer. Both flame spectrometric methods are more sensitive than the standard colorimetric method, but quantification is easier for the atomic fluorescence method. The latter technique has a wide linear dynamic range and is unaffected by a gradual increase in the residual H₂S level in the system. The atomic fluorescence signal is also unaffected by the presence of volatile hydrocarbons in the sewage. The results obtained with the fluorescence method agree well with those obtained with the standard method, while the flame photometric results are low. Studies on the effect of metal ions on the fluorescence signal indicate that the method determines “total sulfide”.     

Mechanisms of mineral scaling in oil and geothermal wells studied in laboratory experiments by nuclear techniques

Two independent nuclear methods have been developed and tested for studies of mineral scaling mechanisms and kinetics related to the oil and geothermal industry. The first is a gamma transmission method to measure mass increase with a 30 MBq source of ¹³³Ba. The other method applies radioactive tracers of one or more of the scaling components. CaCO₃-precipitation has been used as an example here where the main tracer has been ⁴⁷Ca²⁺. While the transmission method is an indirect method, the latter is a direct method where the reactions of specific components may be studied. Both methods are on-line, continuous and non-destructive, and capable to study scaling of liquids with saturation ratios approaching the solubility product. A lower limit for detection of CaCO₃ with the transmission method in sand-packed columns with otherwise reasonable experimental parameters is estimated to be <1 mg in a 1 cm section of the tube packed with silica sand while the lower limit of detection for the tracer method with reasonable experimental parameters is estimated to <1 μg in the same tube section.     

Quantitative method for determining the angles of deflection of light rays reconstructed from the hologram of a phase object

A quantitative method is proposed to study the reconstructed wave front from a single hologram of a phase object. The method is designed to study coarse inhomogeneities in phase objects. Results of an experimental test of this method, confirming its efficiency, are presented. Zh. Tekh. Fiz. 67, 39–42 (March 1997)     

Hyperbolification of dynamical systems: The case of continuous-time systems

We present a new method to generate chaotic hyperbolic systems. The method is based on the knowledge of a chaotic hyperbolic system and the use of a synchronization technique. This procedure is called hyperbolification of dynamical systems. The aim of this process is to create or enhance the hyperbolicity of a dynamical system. In other words, hyperbolification of dynamical systems produces chaotic hyperbolic (structurally stable) behaviors in a system that would not otherwise be hyperbolic. The method of hyperbolification can be outlined as follows. We consider a known n-dimensional hyperbolic chaotic system as a drive system and another n-dimensional system as the response system plus a feedback control function to be determined in accordance with a specific synchronization criterion. We then consider the error system and apply a synchronization method, and find sufficient conditions for the errors to converge to zero and hence the synchronization between the two systems to be established. This means that we construct a 2n-dimensional continuous-time system that displays a robust hyperbolic chaotic attractor. An illustrative example is given to show the effectiveness of the proposed hyperbolification method.     

Optimal design method for magnetization directions of a permanent magnet array

In many magnetic systems, the permanent magnet (PM) pattern has a great influence on their performance. This study proposes a systematic optimization method for designing discrete magnetization directions. While previous works have been mostly dependent on researchers’ intuition, the developed method is systematic and can be applied to a two-dimensional PM-type eddy current brake model. The effectiveness of the method is confirmed, where the design’s aim is to maximize the braking force on a moving conductor. The sensitivity analysis is accomplished by the adjoint variable method and the sequential linear programming is used as an optimizer. Several optimization results for various conditions through the proposed design method are compared to each other and the optimal magnet configuration for an eddy current brake is suggested.     

A Spectrophotometric Method for the Determination of Buclizine Hydrochloride Using the Charge-Transfer Spectrum of Buclizine-Iodine Complex

Abstract

A simple and sensitive spectrophotometric method is described for the determination of buclizine hydrochloride in bulk and tablets form. The method is based on the formation of charge-transfer complex between buclizine, as n-donor, and iodine, as Δ acceptor, which measured spectrophotometrically at 295 and 355 nm. A Job's plot indicated a 1:1 complex between the drug and iodine and Beer's law was obeyed in a concentration range of 4–30 μg ml^?1. A more detailed investigation of the complex was made with respect to its association constant and the free energy change. The method is simple and sensitive and has been applied successfully to the analysis of laboratory-made tablets without any interference from the tablet excipients. To validate the method, the results obtained were compared statistically with a newly developed uv-derivative spectrophotometric method. The charge-transfer method was favored due to its higher sensitivity, cheap coast and available equipments.     

Measurement of the light pressure and energy of a laser pulse

A method is described for measuring the light pressure and energy of a laser pulse. The method is based on a transformation of the kinetic energy acquired by a suspended object from the laser pulse into the potential energy of a twisted elastic filament. Comparative measurements are made of the energy radiated by a pulsed ruby laser ( = 6943 Å) by a calorimetric method and by a method based on measurement of the light pressure. This latter method essentially eliminates the influence of the radiometric effect on the measured results. It permits a quite accurate measurement of the light pressure and energy of a laser pulse at pressures of the order of 10^–5 torr and below.Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, Vol.12, No. 6, pp. 48–54, June, 1969.     

Focal region fields of three dimensional Gregorian system

Maslov’s method is applied to derive high frequency field expressions for the wave reflected by a three dimensional Gregorian system when the plane wave is incident. Expression is relatively simple and is valid in the caustic region. Geometrical optics approximation generally used to study high frequency field, fails in the vicinity of a caustic. Maslov’s method is a systematic procedure for predicting the field in the caustic region combining the simplicity of ray and generality of the transform method. Field distributions around the caustic region are calculated and the results are compared with obtained using current distribution method. Agreement among them is fairly good.