Grain size,strain rate,and temperature dependence of flow stress in ultra-fine grained and nanocrystalline Cu and Al: Synthesis,experiment, and constitutive modeling

For the first time, high quality bulk nanocrystalline (nc) fcc metals, with least amounts of imperfections, exhibiting high strength and ductility at room and different temperatures, under quasi-static and dynamic types of loading, were prepared and a comprehensive study on their post-yield mechanical properties was performed. This investigation included study of the effect of temperature on stress–strain responses of mechanically milled bulk nc Cu and Al. The samples after preparation through mechanical milling and consolidation processes were subjected to uniaxial compressive loading at quasi-static and dynamic strain rates of 10⁻² s⁻¹ and 1840–3105 s⁻¹, respectively, at temperatures ranging from 223 to 523 K. In both materials strong dependency of flow stress to temperature was observed; this dependency was rather more pronounced when the materials were tested at the quasi-static strain rate. Further, a new grain size and temperature dependent viscoplastic phenomenological constitutive equation, Khan–Liang–Farrokh (KLF) model was developed based on the Khan–Huang–Liang (KHL) constitutive equation. The model was featured to correlate different characteristic behaviors of polycrystalline materials in the plastic regime, as the result of grain refinement. In addition, the viscoplastic responses of bulk Cu and Al of different grain sizes (from sub-micron to nanometer range), and those from bulk nc Cu and Al at different strain rates (quasi-static to dynamic), recently published (21 and 22), were simulated using the newly developed equation. The results confirmed reasonable capability of the developed model to correlate a wide spectrum of the viscoplastic responses of these fcc metals.     

Mechanics of the rate-dependent elastic–plastic deformation of glassy polymers from low to high strain rates

A combined experimental and analytical investigation has been performed to understand the mechanical behavior of two amorphous polymers—polycarbonate and poly(methyl methacrylate)—at strain rates ranging from 10⁻⁴ to 10⁴ s⁻¹. This range in strain rates was achieved in uniaxial tension and compression tests using a dynamic mechanical analyzer (DMA), a servo-hydraulic testing machine, and an aluminum split-Hopkinson pressure bar. DMA tension tests were used to characterize the viscoelastic behavior of these materials, with focus on the rate-dependent shift of material transition temperatures. Uniaxial compression tests on the servo-hydraulic machine (10⁻⁴ to 1 s⁻¹) and the split-Hopkinson pressure bar (10³ to 10⁴ s⁻¹) were used to characterize the rate-dependent yield and post-yield behavior. Both materials were observed to exhibit increased rate sensitivity of yield under the same strain rate/temperature conditions as the β-transition of the viscoelastic behavior. A physically based constitutive model for large strain deformation of thermoplastics was then extended to encompass high-rate conditions. The model accounts for the contributions of different molecular motions which become operational and important in different frequency regimes. The new features enable the model to not only capture the transition in the yield behavior, but also accurately predict the post-yield, large strain behavior over a wide range of temperatures and strain rates.     

聚碳酸酯的高应变率拉伸实验

为了解应变率对聚碳酸酯拉伸力学行为的影响,在旋转盘式间接杆杆型冲击拉伸试验机和MTS809材料试验机上,对聚碳酸酯棒材进行了高应变率和准静态加载下的单向拉伸试验,应变率分别为380 s-1、800 s-1、1750 s-1和0.001 s-1、0.05 s-1,得到了聚碳酸酯的拉伸应力应变曲线.试验结果表明:聚碳酸酯的拉伸力学性能具有明显的应变率相关性,其屈服应力和失稳应变随应变率的增加而增大.依据试验结果,采用朱王唐粘弹性本构模型来描述聚碳酸酯的非线性粘弹性拉伸力学行为.模型结果显示,在本文实施的应变率范围内,朱王唐模型可以较好地表征聚碳酸酯的拉伸应力应变响应.     

Multiaxial and non-proportional loading responses,anisotropy and modeling of Ti–6Al–4V titanium alloy over wide ranges of strain rates and temperatures

Results from a series of multiaxial loading experiments on the Ti–6Al–4V titanium alloy are presented. Different loading conditions are applied in order to get the comprehensive response of the alloy. The strain rates are varied from the quasi-static to dynamic regimes and the corresponding material responses are obtained. The specimen is deformed to large strains in order to study the material behavior under finite deformation at various strain rates. Torsional Kolsky bar is used to achieve shear strain rates up to 1000 s⁻¹. Experiments are performed under non-proportional loading conditions as well as dynamic torsion followed by dynamic compression at various temperatures. The non-proportional loading experiments comprise of an initial uniaxial loading to a certain level of strain followed by biaxial loading, using a channel-type die at various rates of loadings. All the non-proportional experiments are carried out at room temperature. Experiments are also performed to investigate the anisotropic behavior of the alloy. An orthotropic yield criterion [proposed by Cazacu, O., Plunkett, B., Barlat, F., 2005. Orthotropic yield criterion for hexagonal closed packed metals. International Journal of Plasticity 22, 1171–1194.] for anisotropic hexagonal closed packed materials with strength differential is used to generate the yield surface. Based on the definition of the effective stress of this yield criterion, the observed material response for the different loading conditions under large deformation is modeled using the Khan–Huang–Liang (KHL) equation assuming isotropic hardening. The model constants used in the present study, were pre-determined from the extensive uniaxial experiments presented in the earlier paper [Khan, A.S., Suh, Y.S., Kazmi R., 2004. Quasi-static and dynamic loading responses and constitutive modeling of titanium alloys. International Journal of Plasticity 20, 2233–2248]. The model predictions are found to be extremely close to the observed material response.     

Microstructure-sensitive modeling of polycrystalline IN 100

A rate dependent, microstructure-sensitive crystal plasticity model is formulated for correlating the mechanical behavior of a polycrystalline Ni-base superalloy IN 100 at 650 °C. This model has the capability to capture first order effects on the stress–strain response due to (a) grain size, (b) γ′ precipitate size distribution, and (c) γ′ precipitate volume fraction. Experimental fatigue data with variable strain rates are used to calibrate the model for several distinct IN 100 microstructures (grain size, precipitate size distributions and volume fractions) obtained from thermomechanical processing. Physically based hardening laws are employed to evolve the dislocation densities for each slip system, taking into consideration the dislocation interaction mechanisms.     

Analysis of heterogeneous deformation and dislocation dynamics in single crystal micropillars under compression

The size dependent deformation of Cu single crystal micropillars with thickness ranging from 0.2 to 2.5 μm subjected to uniaxial compression is investigated using a Multi-scale Dislocation Dynamics Plasticity (MDDP) approach. MDDP is a hybrid elasto-viscoplastic simulation model which couples discrete dislocation dynamics at the micro-scale (software micro3d) with the macroscopic plastic deformation. Our results show that the deformation field in these micropillars is heterogeneous from the onset of plastic flow and is confined to few deformation bands, leading to the formation of ledges and stress concentrations at the surface of the specimen. Furthermore, the simulation yields a serrated stress–strain behavior consisting of discrete strain bursts that correlates well with experimental observations. The intermittent operation and stagnation of discrete dislocation arms is identified as the prominent mechanism that causes heterogeneous deformation and results in the observed macroscopic strain bursts. We show that the critical stress to bow an average maximum dislocation arm, whose length changes during deformation due to pinning events, is responsible for the observed size dependent response of the single crystals. We also reveal that hardening rates, similar to that shown experimentally, occur under relatively constant dislocation densities and are linked to dislocation stagnation due to the formation of entangled dislocation configuration and pinning sites.     

Anisotropic responses, constitutive modeling and the effects of strain-rate and temperature on the formability of an aluminum alloy

Finite deformation anisotropic responses of AA5182-O, over a wide range of strain-rates (10⁻⁴ to 10⁰ s⁻¹) and temperatures (293-473 K) are presented. The plastic anisotropy parameters were experimentally determined from tensile experiments using specimens from sheet material. Using the experimental results under plane stress conditions, the anisotropy coefficients for Barlat’s yield function (YLD96) were calculated at different strain-rates and temperatures. The correlations obtained from YLD96 are in good agreement with the observed experimental results. The strain-rate sensitivity of AA5182-O alloy changed from negative at 293 K to positive at 473 K. Khan-Huang-Liang (KHL) constitutive model is shown to correlate the observed strain-rate and temperature dependent responses reasonably well. The material parameters were obtained from the experimental responses along the rolling direction (RD) of the sheet. Marciniak and Kuckzinsky (M-K) theory was used to obtain the theoretical strain and stress-based forming limit curves (FLCs) at different strain-rates and temperatures. The experimental result from the published literature is compared with the FLCs from the current study.     

A generalized anisotropic hardening rule based on the Mroz multi-yield-surface model for pressure insensitive and sensitive materials

In this paper, a generalized anisotropic hardening rule based on the Mroz multi-yield-surface model for pressure insensitive and sensitive materials is derived. The evolution equation for the active yield surface with reference to the memory yield surface is obtained by considering the continuous expansion of the active yield surface during the unloading/reloading process. The incremental constitutive relation based on the associated flow rule is then derived for a general yield function for pressure insensitive and sensitive materials. Detailed incremental constitutive relations for materials based on the Mises yield function, the Hill quadratic anisotropic yield function and the Drucker–Prager yield function are derived as the special cases. The closed-form solutions for one-dimensional stress–plastic strain curves are also derived and plotted for materials under cyclic loading conditions based on the three yield functions. In addition, the closed-form solutions for one-dimensional stress–plastic strain curves for materials based on the isotropic Cazacu–Barlat yield function under cyclic loading conditions are summarized and presented. For materials based on the Mises and the Hill anisotropic yield functions, the stress–plastic strain curves show closed hysteresis loops under uniaxial cyclic loading conditions and the Masing hypothesis is applicable. For materials based on the Drucker–Prager and Cazacu–Barlat yield functions, the stress–plastic strain curves do not close and show the ratcheting effect under uniaxial cyclic loading conditions. The ratcheting effect is due to different strain ranges for a given stress range for the unloading and reloading processes. With these closed-form solutions, the important effects of the yield surface geometry on the cyclic plastic behavior due to the pressure-sensitive yielding or the unsymmetric behavior in tension and compression can be shown unambiguously. The closed form solutions for the Drucker–Prager and Cazacu–Barlat yield functions with the associated flow rule also suggest that a more general anisotropic hardening theory needs to be developed to address the ratcheting effects for a given stress range.     

Prediction of 42CrMo steel flow stress at high temperature and strain rate

The compressive deformation behavior of 42CrMo steel was investigated at temperatures ranging from 850 to 1150 °C and strain rates from 0.01 to 50 s⁻¹ on Gleeble-1500 thermo-simulation machine. Based on the classical stress–dislocation relation and the kinematics of the dynamic recrystallization, the flow stress constitutive equations of the work hardening-dynamical recovery period and dynamical recrystallization period were established for 42CrMo steel, respectively. The stress–strain curves of 42CrMo steel predicted by the established models are in good agreement with experimental results when the strain rate is relatively low. So, the proposed deformation constitutive equations can be used to establish the hot formation processing parameters for 42CrMo steel.     

A new unified constitutive model with short- and long-range back stress for lead-free solders of Sn–3Ag–0.5Cu and Sn–0.7Cu

A series of tensile tests of Sn–3Ag–0.5Cu and Sn–0.7Cu lead-free solders were investigated at various strain rates from 1 × 10⁻⁴ s⁻¹ to 1 × 10⁻² s⁻¹ and over a wide temperature range from 25 ^oC to 150 ^oC. Two-step strain rate jump tests, three-step short term creep tests with stress jump, and uniaxial ratcheting tests were also conducted. Based on the test data, a new constitutive model was proposed with a simple formulation and only eight material constants which can be easily obtained. The model employs two carefully defined back stress components to simulate the loading/unloading asymmetry phenomenon in uniaxial ratcheting tests. Different evolution rules of short-range back stress were given for loading and unloading stage, which provides the model ability to simulate the asymmetry in hysteresis loops. The proposed model presents good simulation of uniaxial tensile tests, strain rate jump tests, short term creep tests with stress jump, and uniaxial ratcheting tests.     

Strength criterion and elastoplastic constitutive model of frozen silt in generalized plastic mechanics

Triaxial compressive tests of frozen silt were carried out under confining pressures from 0.0 to 14.0 MPa at the temperatures of −2, −4 and −6 °C. A strength criterion based upon experimental results is presented by the combination of extended Lade–Duncan strength function f_π(θ) in π-plane and f_p–q(p) in p–q-plane. In order to describe the deformation characteristic of frozen silt, an elastoplastic constitutive model in generalized plastic mechanics has been proposed for the nonlinear behavior of frozen silt, such as the pressure melting and crushing phenomena, strain softening/hardening characteristics and dilatation, etc., by employing an elliptical yield surface, together with a non-associated flow rule for the compressive mechanism, and two parabolic yield surfaces, together with non-associated flow rules for the shear mechanism. The validity of the model is verified by comparing its modeling results with the results of triaxial compressive tests. It is found that the stress–strain curves predicted by this model agree well with the corresponding experimental results both under low and high confining pressures.     

Yield criterion and elasto-plastic damage constitutive model for frozen sandy soil

A series of triaxial compression tests was carried out on a frozen sandy soil under confining pressures of 0–18 MPa at −6 °C. The experimental results indicate that, the strength of frozen sandy soil increases versus the increase in the confining pressures when σ₃ ? 3 MPa, but decreases when σ₃ > 3 MPa. This phenomenon is called the strengthening and weakening effects of confining pressures. A yield function, considering both effects, is proposed using the experimental method according to Drucker’s postulate, and the mathematical expression of the hardening parameter, which can describe the softening and hardening phenomenon, is provided. An elasto-plastic constitutive model for frozen sandy soil is developed. Based on the continuum damage theory, the cross anisotropic damage variables are deduced and their change regularities are investigated. Then the elasto-plastic damage constitutive model is proposed by introducing damage variables into elasto-plastic constitutive model. The validity of the model is verified by comparing its modeling results with experimental results obtained from triaxial tests. It is found that, this model can predict the deformation regularity of frozen soil exactly. It can simulate the stress–strain process under high confining pressures when pressure melting phenomena appear especially well.     

Thermo-mechanical response of Al 6061 with and without equal channel angular pressing (ECAP)

The thermo-mechanical responses of Al 6061 before and after equal channel angular pressing (ECAP) at different strain rates and temperatures were measured. Al 6061 was solution heat treated before ECAP pressing at room temperature and subjected to up to three passes. After pressing, the billets were aged at 100 °C for 2 days. An as-received Al 6061-T651 was studied similarly to investigate the differences between processed and non-processed specimens. The responses of ECAP material were determined at −30, 22, 125 and 250 °C, and at strain rates from 10⁻⁵ to 2530 s⁻¹; the 6061-T651 specimens were subjected to uniaxial compressive loading at −31, 22, 85, 150, 230 and 315 °C, and strain rates ranging from 10⁻⁵ to 2200 s⁻¹. It was found that, the ECAP process increases the strength versus the T651 condition. Additionally, the Al 6061 ECAP is not sensitive to strain rate at room and lower temperatures, but the sensitivity increases as the number of passes and/or temperature are increased and this is the same for the non-processed material. Increasing the number of passes increases the flow stress at room and lower temperatures, has almost no effect at 125 °C and decreases at 250 °C. For both materials, the dynamic flow stress is higher than the stress at quasi-static strain rates even when the quasi-static strain rate regime is insensitive to strain rate. The Al 6061 has strong texture after one pass but steadily increases as the number of passes are increased. This is the first study that reports on the thermo-mechanical responses of ECAP and non-ECAP Al 6061 at such a wide range of strain rates, including dynamic, and temperatures.     

Experimental investigation of cyclic and time-dependent deformation of titanium alloy at elevated temperature

A novel cyclic deformation test program was undertaken to characterize macroscopic time dependent deformation of a titanium alloy for use in viscoplastic model development. All tests were conducted at a high homologous temperature, 650 °C, where there are large time dependent and loading rate dependent effects. Uninterrupted constant amplitude tests having zero mean stress or a tensile mean stress were conducted using three different control modes: strain amplitude and strain rate, stress amplitude and stress rate, and a hybrid stress amplitude and strain rate. Strain ratcheting occurred for all cyclic tests having a tensile mean stress and no plastic shakedown was observed. The shape of the strain ratcheting curve as a function of time is analogous to a creep curve having primary, steady state and tertiary regions, but the magnitude of the ratchet strains are higher than creep strains would be for a constant stress equal to the mean stress. Strain cycles interrupted with up to eight 2-h stress relaxation periods around the hysteresis loop, including hold times in each quadrant of the stress–strain diagram, were also conducted. Stress relaxation was path-dependent and in some cases the stress relaxed to zero. The cyclic behavior of these interrupted tests was similar even though each cycle was very complex. These results support constitutive model development by providing exploratory, characterization and validation data.     

The effect of time-dependent twinning on low temperature (<0.25 ∗ Tm) creep of an alpha-titanium alloy

The low-temperature (less than one-fourth of the melting temperature) creep deformation behavior of hexagonally close-packed (HCP) α-Ti–1.6 wt.% V was investigated. Creep tests were performed at various temperatures between room temperature and 205 °C at 95% of the respective yield stress at the different temperatures. The creep strain rate was found to increase with increasing temperature. Scanning and transmission electron microscopy revealed that slip and unusually slow twin growth, or time-dependent twinning, are active deformation mechanisms for the entire temperature range of this investigation. The activation energy for creep of this alloy was calculated to identify the rate-controlling deformation mechanism, and was found to increase with increasing creep strain. At low strain, the activation energy for creep was found to be close to the previously calculated activation energy for slip. At high strain, the calculated activation energy indicates that both slip and twinning are significant deformation mechanisms. The appearance of twinning at high strains is explained by a model for twin nucleation by dislocation pileups.     

A Micromechanics Study of Lamellar TiAl

Microdeformation patterns of lamellar TiAl specimens with various grain sizes under uniaxial tension are mapped using the micro/nano experimental mechanics technique called SIEM (Speckle Interferometry w ith Electron Microscopy). The stress–strain relationships were obtained from deformations within decreasing areas ranging from mm² to μm². We found that the stress–strain relationship of the material depends on the size of strain measuring area in relation to the grain size. The stiffness at a grain boundary can be as large as 7–10 times more than that of the grain itself. From the data obtained so far, it seems that the traditional way of using PST (polysynthetically twinned) single crystal to predict polycrystalline behavior may not be appropriate.     

Modelling large deformation behaviour under loading–unloading of semicrystalline polymers: Application to a high density polyethylene

In this work, the large deformation behaviour under monotonic loading and unloading of a high density polyethylene (HDPE) is studied. To analyze the nonlinear time-dependent response of the material, mechanical tests were conducted at room temperature under constant true strain rates and stress relaxation conditions. A physically-based inelastic model written under finite strain formulation is proposed to describe the mechanical behaviour of HDPE. In the model, the inelastic mechanisms involve two parallel elements: a visco-hyperelastic network resistance acting in parallel with a viscoelastic–viscoplastic intermolecular resistance where the amorphous and crystalline phases are explicitly taken into consideration. The semicrystalline polymer is considered as a two-phase composite. The influence of the crystallinity on the loading and unloading behaviour is investigated. Numerical results are compared to experimental data. It is shown that the model is able to accurately reproduce the experimental observations corresponding to monotonic loading, unloading and stress relaxation behaviours at different strain levels. Finally, the model capabilities to capture cyclic loading–unloading behaviour up to large strains are discussed. To demonstrate the improved modelling capabilities, simulations are also performed using the original model of Boyce et al. [Boyce, M.C., Socrate, S., Llana, P.G., 2000. Constitutive model for the finite deformation stress–strain behavior of poly(ethylene terephthalate) above the glass transition. Polymer 41, 2183–2201] modified by Ahzi et al. [Ahzi, S., Makradi, A., Gregory, R.V., Edie, D.D., 2003. Modeling of deformation behavior and strain-induced crystallization in poly(ethylene terephthalate) above the glass transition temperature. Mechanics of Materials 35, 1139–1148].     

Influence of temperature and strain rate on the mechanical behavior of three amorphous polymers: Characterization and modeling of the compressive yield stress

Uniaxial compression stress–strain tests were carried out on three commercial amorphous polymers: polycarbonate (PC), polymethylmethacrylate (PMMA), and polyamideimide (PAI). The experiments were conducted under a wide range of temperatures (−40 °C to 180 °C) and strain rates (0.0001 s⁻¹ up to 5000 s⁻¹). A modified split-Hopkinson pressure bar was used for high strain rate tests. Temperature and strain rate greatly influence the mechanical response of the three polymers. In particular, the yield stress is found to increase with decreasing temperature and with increasing strain rate. The experimental data for the compressive yield stress were modeled for a wide range of strain rates and temperatures according to a new formulation of the cooperative model based on a strain rate/temperature superposition principle. The modeling results of the cooperative model provide evidence on the secondary transition by linking the yield behavior to the energy associated to the β mechanical loss peak. The effect of hydrostatic pressure is also addressed from a modeling perspective.     

Crystal plasticity-based forming limit prediction for non-cubic metals: Application to Mg alloy AZ31B

A viscoplastic crystal plasticity model is incorporated within the Marciniak–Kuczynski (M–K) approach for forming limit curve prediction. The approach allows for the incorporation of crystallographic texture-induced anisotropy and the evolution of the same. The effects of mechanical twinning on the plastic response and texture evolution are also incorporated. Grain-level constitutive parameters describing the temperature dependent behavior of hexagonal close packed Mg alloy, AZ31B, sheets at discrete temperatures are used as a first application of the model. A trade-off between significant strain hardening behavior at lower temperatures (∼150 °C), and significant strain rate hardening at higher temperatures (∼200 °C) lead to similarities in the predicted forming limits. The actual formability of this alloy depends strongly on temperature within this range, and this distinction with the current modeling is related to more localized instability-based failure mechanisms at the lower temperatures than is assumed in the M–K approach. It is shown that the strain path dependence in the strain hardening response is significant and that it influences the forming limits in a predictable way. For broader applicability, a means of incorporating dynamic recrystallization into the crystal plasticity model is required.     

A Technique for Dynamic Tensile Testing of Human Cervical Spine Ligaments

An experimental study is undertaken to examine the dynamic stress–strain characteristics of ligaments from the human cervical spine (neck). Tests were conducted using a tensile split Hopkinson bar device and the engineering strain rates imposed were of the order of 10²∼10³/s. As ligaments are extremely soft and pliable, specialized test protocols applicable to Hopkinson bar testing were developed to facilitate acquisition of reliable and accurate data. Seven primary ligaments types from the cervical spines of three male cadavers were subjected to mechanical tests. These yielded dynamic stress–strain curves which could be approximated by empirical equations. The dynamic failure stress/load, failure stain/deformation, modulus/stiffness, as well as energy absorption capacity, were obtained for the various ligaments and classified according to their location, the strain rate imposed and the cadaveric source. Compared with static responses, the overall average dynamic stress–strain behavior foreach type of ligament exhibited an elevation in strength but reduced elongation.