Hybrid stress analysis by digitized photoelastic data and numerical methods

A method is presented that determines photoelastic isochromatic values at the nodal points of a grid mesh which in turn is generated by a computer program that accepts digitized input. Values of σ₁ - σ₂ are computed from the digitized fringe orders. The Laplace equation is solved to separate the principal stresses at each nodal point. The method is extended to digitize isoclinics. Subsequently, σ _x - σ _y and τ _xy are calculated to be used as starting values for the solution of the pertaining partial differential equations to enhance convergence. For further accelerating the rate of convergence, superfluous boundary conditions are added from the digitized data; significant improvement is demonstrated. Estimated values of σ _x - σ _y from the digitized data are further used in conjunction with the solution of the Laplace equation to determine the state of stress without solving the boundary value problems. Paper was presented at the 1988 SEM Spring Conference on Experimental Mechanics held in Portland, OR on June 5–10.     

Fatigue gage utilizing slip-initiation phenomenon in electroplated copper foil

Fundamental experiments are carried out to examine the parameter that dominates the slip-band initiation in electroplated copper foil under the condition where the mean stress as well as the stress amplitude varies. In the case of constant-amplitude stressing, the relation between the critical stress for the slip-band initiation σ _p and the number of cyclesN is well represented by σ _p ^α N=C. In other words, the slip bands appear when the total hysteresis energy applied to the copper foil attains a critical value. In the case of variable stresses, the range-pair mainly dominates the occurrence of the slip bands, and Miner's linear cumulative damage rule holds for the accumulation of the fatigue damage for the slip-band initiation. Accordingly, the parameter (Σσ _i ^α n _i/Σn _i)^1/α is equivalent to the critical stress σ _p under constant amplitude stressing, where σ _i andn _i are the stress amplitude and the number of cycles counted by the range-pair method, respectively, and α is the exponent of the σ _p -N relation. Based on these results, the applicability of the copper foil to the fatigue gage that accumulates and indicates a load experience is discussed.     

Influence of molecular parameters on the stress dependence of viscous and elastic properties of polypropylene melts in shear

The stress dependencies of the steady-state viscosity η and, particularly, that of the steady-state elastic compliance J _e of various linear isotactic polypropylenes (PP) and one long-chain branched PP are investigated using creep-recovery tests. The creep stresses applied range from 2 to 10,000 Pa. In order to discuss the stress-dependent viscosity η and elastic compliance J _e with respect to the influence of the weight average molar mass M _w and the polydispersity factor M _w/M _n the PP are characterized by SEC–MALLS. For the linear PP, linear steady-state elastic compliances J_e⁰J_{\rm e}^0 in the range of 10^− 5–10^− 3 Pa^− 1 are obtained depending on the molar mass distribution. J_e⁰J_{\rm e}^0 of the LCB-PP is distinctly higher and comes to lie at around 10^− 2 Pa^− 1. J_e⁰J_{\rm e}^0 is found to be independent of M _w but strongly dependent on polydispersity. η and J _e decrease with increasing stress. For the linear PP, J _e as a function of the stress τ is temperature independent. The higher M _w/M _n the stronger is the shear thinning of η and the more pronounced is the stress dependence of J _e. For the LCB-PP, the strongest stress dependence of η and J _e is observed. Furthermore, for all PP J _e reacts more sensitively to an increasing stress than η. A qualitative explanation for the stronger stress dependence of J _e compared to η is given by analyzing the contribution of long relaxation times to the viscosity and elasticity.     

A new apparatus for studying mechanical behavior under pressure

Using a servohydraulic intensifier, a servohydraulic universal test machine and a novel test chamber, pressures of 750 MPa and axial stresses of almost any magnitude are simultaneously generated and applied to the gage section of a solid, cylindrical specimen. Under combined axial-stress/external-pressure loadings, a solid specimen experiences a truly three-dimensional, homogeneous stress state in which the axial stress equals σ₁ and the radial and circumferential stresses equal the negative of the pressure, —P. Through independent computer control of the pressure and axial stress, amterial behavior under monotonically and cyclically applied multiaxial stresses are investigated. This paper describes the experimental details of the test chamber design, high-pressure fluid production and sealing, load and strain measurement under high pressure, computer control and data acquisition. Experimental results obtained from triaxial monotonic tests on low alloy steel and triaxial cyclic tests on a Ni-Ti alloy using this unique apparatus are presented.     

Molecular dynamics studies on the dislocation gliding near a tilt boundary

The gliding behavior of edge dislocation near a grain boundary (GB) in copper under pure shear stresses is simulated by using molecular dynamics(MD) method. Many-body potential incorporating the embedded atom method (EAM) is used. The critical shear stresses for a single disocation to pass across GB surface are obtained at values of σ _c =23MPa ∼ 68 MPa and 137MPa∼274 MPa for Ω=165 small angle tilt GB at 300K and 20K, respectively. The first result agrees with the experimental yield stress σ _y (=42MPa) quite well. It suggests that there might be one of the reasons of initial plastic yielding caused by single dislocation gliding across GB. In addition, there might be possibility to obtain yield strength from microscopic analysis. Moreover, the experimental value of σ _y at low temperature is generally higher than that at room temperature. So, these results are in conformity qualitatively with experimental fact. On the other hand, the Ω=25 GB is too strong an obstacle to the dislocation. In this case, a dislocation is able to pass across GB under relatively low stress only when it is driven by other dislocations. This is taken to mean that dislocation pile-up must be built up in front of this kind of GB, if this GB may take effect on the process of plastic deformation. The project supported by KM85-33 of Academia Sinica and the National Natural Science Foundation of China     

Axial crack propagation and arrest in a pressurized cylinder: An experimental-numerical analysis

The feasibility of using a previously developed crack-kinking criterion to predict crack arrest at a tear strap in a pressurized fuselage was studied with instrumented axial rupture tests of 21 models of an idealized fuselage. A rapidly propagating axial crack, which was initiated from a precrack, kinked immediately upon extension and propagated diagonally until it turned circumferentially and propagated along the tear straps. An elastodynamic finite element analysis of the rupturing model fuselage yielded the mixed-mode stress intensity factors,K _I andK _II , and the remote stress component, σ _OX . This numerical procedure was also used to predict the crack trajectories in full-scale fuselage rupture tests. All numerical results agreed well with their measured counterparts regardless of size.     

Range-pair-counting fatigue gage

In this paper, the surface roughening phenomenon of an aluminum foil during fatigue process is utilized for monitoring of a variable amplitude stress. It is found that constant mean stress does not affect surface roughness. When the mean stress varies, however, it causes surface roughening. In such a case, the equivalent stress defined by (Σσ _i ^α N _i /ΣN _i )^1/α dominates surface roughness of an aluminum foil, where σ _i andN _i are stress amplitude and the number of cycles counted by the rangepair method, respectively, and α is a gage factor which is peculiar to the foil used. It is concluded that the aluminum foil can be used as the range-pair counting fatigue gage with high accuracy.     

The effect of residual stresses on hardness measurements

The RockwellC hardness,RC, was measured as a function of position on steel rings with different residual-stress profiles through the thickness. An experimental correlation between residual stress andRC was obtained. A relationship between the average pressurep of a spherical indenter, the yield strengthS _y and the residual stress of the material was conceived and used in fitting the experimental data. In order to model the effects of residual stresses on the measured hardness, the von Mises-Hencky (power) yield criterion was utilized, together with an adaptation for residual stresses of the expression for the stress state under a spherical indenter, given in Shaw, Hoshi and Henry. A parameter α was introduced in our calculations to account for the effect of the nonperpendicularity of the residual stresses to the pressurep of the spherical indenter. The proposed model in large measure fits experimental hardness versus residual stress data, and results are consistent with different samples. This model can be used as a basis for the measurement of residual stresses in steel or other materials.     

Prediction of mixed-mode fracture based on an elasto–plastic energy balance criterion

The maximum energy release rate criterion, i.e., G _max criterion, is commonly used for crack propagation analysis. This fracture criterion is based on the elastic macroscopic strength of materials. In the present investigation, however, the G _max criterion has been modified in order to accommodate the consideration of plastic strain energy. This modified criterion is extended to study the fatigue crack growth characteristics of mixed-mode cracks. To predict crack propagation due to fatigue loads, a new elasto–plastic energy model is presented. This new model includes the effects of material properties such as strain hardening exponent n, yield strength σ _y , and fracture toughness and stress intensity factor ranges. The results obtained are compared with those obtained using the commonly employed crack growth law and the experimental data.     

Nonlinear rheology of concentrated spherical silica suspensions: 3. Concentration dependence

Nonlinear rheology was examined for concentrated suspensions of spherical silica particles (with radius of 40 nm) in viscous media, 2.27/1 (wt/wt) ethylene glycol/glycerol mixture and pure ethylene glycol. The particles were randomly and isotropically dispersed in the media in the quiescent state, and their effective volume fraction φ_eff ranged from 0.36 to 0.59. For small strains, the particles exhibited linear relaxation of the Brownian stress σ_B due to their diffusion. For large step strains γ, the nonlinear relaxation modulus G(t,γ) exhibited strong damping and obeyed the time-strain separability. This damping was related to γ-insensitivity of strain-induced anisotropy in the particle distribution that resulted in decreases of σ_B/γ. The damping became stronger for larger φ_eff. This φ_eff dependence was related to a hard-core volume effect, i.e., strain-induced collision of the particles that is enhanced for larger φ_eff. Under steady/transient shear flow, the particles exhibited thinning and thickening at low and high γ˙, respectively. The thinning behavior was well described by a BKZ constitutive equation using the G(t,γ) data and attributable to decreases of a Brownian contribution, σ_B/γ˙. The thickening behavior, not described by this equation, was related to dynamic clustering of the particles and corresponding enhancement of the hydrodynamic stress at high γ˙. In this thickening regime, the viscosity growth η₊ after start-up of flow was scaled with a strain γ˙t. Specifically, critical strains γ_d and γ_s for the onset of thickening and achievement of the steadily thickened state were independent of γ˙ but decreased with increasing φ_eff. This φ_eff dependence was again related to the hard-core volume effect, flow-induced collision of the particles enhanced for larger φ_eff. Received: 26 June 1998 Accepted: 9 December 1998     

Some features of the buckling of stringer shells

A technique for stability analysis of stringer shells is proposed. It is used to analyze the minimum critical stresses. The dependence of the dimensionless parameters σ_cr/σ_cl on the number of stringers is plotted. The linear and nonlinear theories of ribbed shells are used to examine the features of how stringer shells lose stability. It is shown that the minimum critical stresses determined using the theory of ribbed shells and a structurally orthotropic model are close within the range of stiffness parameters considered __________ Translated from Prikladnaya Mekhanika, Vol. 42, No. 2, pp. 59–64, February 2006.     

Melt shear rheology of carbon nanofiber/polystyrene composites

The rheological behavior and morphology of carbon nanofiber/polystyrene (CNF/PS) composites in their melt phase have been characterized both through experimental measurements and modeling. Composites prepared in the two different processes of solvent casting and melt blending are contrasted; melt-blended and solvent-cast composites were each prepared with CNF loadings of 2, 5, and 10 wt%. A morphological study revealed that the melt blending process results in composites with shorter CNFs than in the solvent-cast composites, due to damage caused by the higher stresses the CNFs encounter in melt blending, and that both processes retain the diameter of the as-received CNFs. The addition of carbon nanofiber to the polystyrene through either melt blending or solvent casting increases the linear viscoelastic moduli, G′ and G″, and steady-state viscosity, η, in the melt phase monotonically with CNF concentration, more so in solvent cast composites with their longer CNFs. The melt phase of solvent-cast composites with higher CNF concentrations exhibit a plateau of the elastic modulus, G′, at low frequencies, an apparent yield stress, and large first normal stress difference, N ₁, at low strain rates, which can be attributed to contact-based network nanostructure formed by the long CNFs. A nanostructurally-based model for CNF/PS composites in their melt phase is presented which considers the composite system as rigid rods in a viscoelastic fluid matrix. Except for two coupling parameters, all material constants in the model for the composite systems are deduced from morphological and shear flow measurements of its separate nanofiber and polymer melt constituents of the composite. These two coupling parameters are polymer–fiber interaction parameter, σ, and interfiber interaction parameter, C _I. Through comparison with our experimental measurements of the composite systems, we deduce that σ is effectively 1 (corresponding to no polymer–fiber interaction) for all CNF/PS nanocomposites studied. The dependence of CNF orientation on strain rate which we observe in our experiments is captured in the model by considering the interfiber interaction parameter, C _I, as a function of strain rate. Applied to shear flows, the model predicts the melt-phase, steady-state viscosities, and normal stress differences of the CNF/PS composites as functions of shear rate, polymer matrix properties, fiber length, and mass concentration consistent with our experimental measurements.     

双均值逼近屈服准则解析含腐蚀缺陷管道爆破压力

通过对Tresca和TSS屈服边长和边心距的均值同时进行逼近,建立了一个线性屈服准则,称为双均值逼近屈服准则.该准则在π平面上是一个等边非等角的十二边形,位于Mises圆内部.利用该准则对受内压作用的管道进行塑性极限分析,导出了含腐蚀缺陷管道爆破压力的解析解.该解析解是管材屈强比(σY/σT)、原始管道厚径比(t0/D0)、抗拉强度σT以及缺陷深度比(d0/t0)的函数.对比表明,该解析解所预测爆破压力与已有模拟和实验数据吻合较好.影响参数的定量分析表明,爆破压力随着屈强比或原始管道厚径比的增大而增大,随着缺陷深度比的增加而减小.所建立的爆破压力解析解对于管道的选材、设计以及安全评估具有重要意义.     

Planar elongation of soft polymeric networks

A new test fixture for the filament stretch rheometer (FSR) has been developed to measure planar elongation of soft polymeric networks with application towards pressure-sensitive adhesives (PSAs). The concept of this new geometry is to elongate a tube-like sample by keeping the perimeter constant. To validate this new technique, soft polymeric networks of poly(propylene oxide) (PPO) were investigated during deformation. Particle tracking and video recording were used to detect to what extent the imposed strain rate and the sample perimeter remained constant. It was observed that, by using an appropriate choice of initial sample height, perimeter, and thickness, the planar stretch ratio will follow l(t) = h(t)/h₀ = exp([(e)\dot] t)\lambda(t) = h(t)/h_0= \exp({\dot{\varepsilon}} t), with h(t) being the height at time t and [(e)\dot]{\dot{\varepsilon}} the imposed constant strain rate. The perimeter would decrease by a few percent only, which is found to be negligible. The ideal planar extension in this new fixture was confirmed by finite element simulations. Analysis of the stress difference, σ _zz  − σ _xx , showed a network response similar to that of the classical neo-Hookean model. As the Deborah number was increased, the stress difference deviated more from the classical prediction due to the dynamic structures in the material. A modified Lodge model using characteristic parameters from linear viscoelastic measurements gave very good stress predictions at all Deborah numbers used in the quasi-linear regime.     

Curing effects on the acoustical properties of epoxy polymers

This paper presents an experimental method for measuring the attenuation and the velocity of longitudinal ultrasonic waves propagating through flat epoxy polymer samples. The study takes place in the first phase of epoxy polymer's polymerization, where these materials pass slowly from liquid state to the solid state. For this purpose an experimental setup was introduced, suitable for the accurate evaluation of the acoustic properties Δα andc _ℓ ^e , when the epoxy polymers are in their first phase of polymerization, while they are cured for 24 hours at room temperature (20°C). The ultrasonic method used is the pulse echo-through transmission technique. From the variation ofc _ℓ ^e and Δα during the first phase of epoxy polymers curing, the three characteristic states: liquid, semi-solid and solid, are clearly determined. It is also observed that plasticizer reduces the testability and the semi-solid state shows greater attenuation than either the liquid or the solid state.     

Vortex ring generation due to the coalescence of a water drop at a free surface

 Results are presented of an experimental investigation of vortex ring formation by a fluid drop contacting a free surface with negligible velocity. The pool fluid is mixed with fluorescein dye, and a laser sheet is used to illuminate a plane of the flow. A series of representative images is recorded by a CCD camera and speculation is made regarding specific sources of vorticity flux through the free surface. Two scaling analyses previously presented by other investigators are demonstrated to be equivalent under the assumptions of this experiment, and they provide the motivation for a series of test runs in which the duration of the coalescence process, τ_*, is related to variations in drop diameter L and fluid surface tension σ. Experimental results are in agreement with the analyses, showing τ_*∼σ^-1/2 and τ_*∼L ^3/2. Received: 22 December 1995 / Accepted: 15 October 1996     

Rheology of lyotropic and thermotropic lamellar phases

We investigate the steady-state rheological behaviour of the lamellar phase of a lyotropic system (CpCl, hexanol, brine) and of a thermotropic system (8CB). Power laws characterize the behaviour of the imposed stress as a function of the measured shear rate and similarities are observed for both systems; the same regime γ˙∼σ ^m with m≈1.7 is obtained at low shear stresses corresponding to a texture of oily streaks oriented in the direction of the flow, as shown by microscopic observations. The “onion state” only exists in the case of dilute samples of the lyotropic lamellar phase; the stress then varies as γ˙∼σ ^m with m≈4.8, as already observed by other groups with different systems. Rheological measurements at different temperatures allow determination of different activation energies relating to the still badly understood processes involved in the different rheological regimes. We propose a model which reproduces the experimental power laws and which is based on an analogy with the theory of high-temperature creep in metals and alloys. Received: 19 October 1999/Accepted: 1 November 1999     

On the orders of the best approximations of integrals of functions by integrals of rank σ

We study the values e _σ(f) of the best approximation of integrals of functions from the spaces L _p (A, dμ) by integrals of rank σ. We determine the orders of the least upper bounds of these values as σ → ∞ in the case where the function ƒ is the product of two nonnegative functions one of which is fixed and the other varies on the unit ball U _p (A) of the space L _p (A, dμ). We consider applications of the obtained results to approximation problems in the spaces S _p ^ϕ. __________ Translated from Neliniini Kolyvannya, Vol. 10, No. 4, pp. 528–559, October–December, 2007.     

A critical review of microscale mechanical testing methods used in the design of microelectromechanical systems

Microelectromechanical systems (MEMS) technologies are evolving at a rapid rate with increasing activity in the design, fabrication, and commercialization of a wide variety of microscale systems and devices. The importance of accurate mechanical property measurement for successful design was realized early on in the development of this field. Consequently, there exist many different techniques to measure quantities such as the Young's modulus (E), yield strength (σ _Y ), fracture strength (σ _F ), residual stress (σ _F ), and residual stress gradient (∇σ _R ) of microscale structures and materials. We review and critically compare several of the important techniques including the microtension test, axisymmetric plate bend test, microbeam bend test, M-test, wafer curvature measurements, dynamic (resonant) tests, fabrication of passive strain sensors, and Raman spectroscopy. We discuss the characteristics of typical test structures, and the common sources of structure-related errors in measurement. A rational approach for the selection of test techniques for the design of microsystems is suggested.