共查询到20条相似文献,搜索用时 15 毫秒
1.
Crystallography Reports - Two complexes with V-shaped ligands, [(L1)2Mn(H2O)4](HSA)2] (1), {[(L1)2Zn(H2O)2](HSA)2}n (2) (L1 = bis(4-(1H-imidazol-1-yl)phenyl)methanone, H2SA = salicylic acid), have... 相似文献
2.
Crystallography Reports - Two coordination polymers, {[L1Zn(adc)]2⋅5H2O}n (1), {[L1Cd(adc)]2⋅2.75H2O}n (2) (L1 = bis(4-(1H-imidazol-1-yl)phenyl)methanone, H2adc =... 相似文献
3.
Crystallography Reports - A cobalt coordination polymer, {[Co(L1)2(H2O)2] · (HCOO)2 · H2O}n, where L1 is a bis(4-(1H-imidazol-1-yl)phenyl)methanone, has been synthesized and characterized... 相似文献
4.
Crystallography Reports - Two novel complexes, {[L1Ni(ipa)(H2O)]2(DMF)}n (1) and {[L1Zn(pa)]4(H2O)}n (2), (L1 = bis(4-(1H-benzo[d]imidazol-1-yl)phenyl)methanone, H2ipa = isophthalic acid, H2pa =... 相似文献
5.
Crystallography Reports - A cobalt coordination polymer with V-shaped ligands, {[Co0.5(L1) ⋅ (C4H2O4)0.5] ⋅ 0.25H2O}n, (L1 = 4-(1H-imidazol-1-yl)phenyl)methanone, C4H2O4 =... 相似文献
6.
Crystallography Reports - A coordination polymer with the V-shaped ligands, {Cd2(bipmo)2(bdc)2?H2O}n (1), (where bipmo is bis(4-(1H-imidazol-1-yl)phenyl)methanone; H2bdc is... 相似文献
7.
8.
Crystallography Reports - A zinc coordination polymer with V-shaped ligands, [L1Zn(npa)]n (L1 = bis(4-(2'-methylimidazol)phenyl)sulfone, H2npa = 4-nitrophthalic acid) has been synthesized under... 相似文献
9.
James E. Johnson Diana C. Canseco Debra D. Dolliver Jeffrey E. Rowe Frank R. Fronczek 《Journal of chemical crystallography》2006,36(10):667-672
Ethyl (2Z)-3-(4-chlorophenyl)-2-cyano-3-(methoxyamino)prop-2-enoate was prepared by reacting the lithium salt of ethyl cyanoacetate with (Z)-O-methyl-4-chloroben-zohydroximoyl fluoride. This compound crystallizes in space group Pbca,with lattice constants a=7.5740(15) ?, b=11.337(2) ?, and c=30.424(5) ? at 110 K. Characterizations include spectrometric identifications employing IR, UV, and 1H and 13C NMR. The compound exists in the solid as the enamine tautomer, with the cyano group cis to the 4-chlorophenyl group (the Z configuration). The C=C and C–N bond distances are 1.3930(16) ? and 1.3278(16) ?, respectively. The N–H group forms a bifurcated hydrogen bond with acceptors C=O (intramolecular) and C≡N (intermolecular).Supplementary material CCDC-289444 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/data_request/cif, by e-mailing data_request@ccdc.cam.ac.uk, or by contacting The Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB2 1EZ, UK; Fax: +44(0)1223-336033. 相似文献
10.
Crystallography Reports - A cobalt coordination polymer with the formula of {[Co(L1)(pa)]}n (1) (L1 = bis(4-(1H-benzo[d]imidazol-1-yl)phenyl)methanone, H2pa = phthalic acid) was synthesized under... 相似文献
11.
Crystallography Reports - The title compound, 1-(4-(5,6-dihydropyridazin-1(4H)-yl)phenyl)-N-methylmethanesulfonamide (C12H17N3O2S), was isolated as an impurity during the preparation of sumatriptan... 相似文献
12.
Crystallography Reports - The Schiff base, 3-(2-(2-hydroxybenzylidene)hydrazinyl)quinoxalin-2(1H)-one has been synthesized by condensation of 3-hydrazinyl quinoxalin-2(1H)-one and salicylaldehyde... 相似文献
13.
9-(4-Nitrophenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H) acridinedione (NTHA) crystallizes in orthorhombic space group P212121 with a = 5.9716(1) Å, b = 18.0476(3) Å, c = 19.2445(2) Å, V = 2074.04(5) Å3, Z = 4, Dcal = 1.263 Mg m?3 and R = 0.0521 (wR = 0.1326) for 4078 observed reflections. 9-(4-Nitrophenyl)-10-(4-methoxyphenyl)-3,3,6,6-tetramethyl-3,4,6,7,9,10-hexahydro-1,8(2H,5H) acridinedione NMTHA, crystallizes in monoclinic space group P21/c with a = 15.669(5) Å, b = 10.652(4) Å, c = 18.337(6) Å, β = 108.25(1)°, V = 2906.66(2) Å3, Z = 4, Dcal = 1.245 Mg m?3 and R = 0.0725 (wR = 0.1847) for 5105 observed reflections. The experimental values are compared with the theoretical values calculated based on the semiemperical methods. The structures are stabilized by N–H?sO and C–H?sO types of intermolecular interactions in addition to van der Waals forces. 相似文献
14.
Cathryn A. Slabber Craig D. Grimmer Orde Q. Munro Ross S. Robinson 《Journal of chemical crystallography》2018,48(4):213-219
The title chalcone, of formula C15H11F1O2, crystallized in the orthorhombic space group P212121 (# 19) with crystal parameters a?=?6.9998(8) Å, b?=?12.6740(15) Å, c?=?12.8997(15) Å, V?=?1144.4(2) Å3, Z?=?4, determined at 100 K with MoKα radiation. The solid-state structure displays an intramolecular S(6) hydrogen bond and the crystal architecture is maintained by intermolecular F?H, O?H, and C?C short contacts. A DFT geometry optimization is compared with the experimental structure. As 19F NMR spectroscopy can be used for metabolic tagging of biologically active compounds (including chalcones), the solution-state 19F chemical shift and 13C19F coupling constants (nJ) are also reported. 相似文献
Graphical Abstract
15.
Crystallography Reports - (E)-4-(2-(4-Cyanobenzylidene)hydrazinyl)benzonitrile dimethyl sulfoxide hemisolvate, C15H10N4 ⋅ 0.5C2H6OS is synthesized following a green protocol and its crystal... 相似文献
16.
Sharma Devinder K. Subbulakshmi K. N. Narayana B. Sarojini B. K. Anthal Sumati Kant R. 《Crystallography Reports》2017,62(7):1148-1151
Crystallography Reports - 2-(4-Chlorophenyl)-3-(phenylamino)-5-(thiophen-2-ylmethylidene)-3,5-dihydro-4H-imidazol-4-one, C20H14N3OSCl was synthesized and its crystal structure was determined by... 相似文献
17.
Yun J. Lee Jason R. King Bala Chandra Chenna Samuel B. OwensJr. Jason L. Freeman Gary M. Gray Sadanandan E. Velu 《Journal of chemical crystallography》2009,39(12):902-907
Abstract
Details of the synthesis and crystal structure determination of (E)-2-(7-(3-(thiophen-2-yl)acrylamido)-2,3-dihydro-5-oxobenzo[e][1,4]oxazepin-1(5H)-yl)ethyl acetate are presented. The compound crystallizes in the triclinic P−1 space group (a = 8.3377(17), b = 9.792(2), c = 12.469(3) ?, α = 96.39(3)°, β = 108.50(3)°, γ = 97.68(3)°, V = 943.9(3) ?3, Z = 2). Interesting features of the structure include intermolecular hydrogen bonding between the amide proton on one molecule and the carbonyl oxygen of the dihydrooxazepinone ring on an adjacent molecule, the boat conformation of the dihydrooxazepinone ring, and π-π stacking between thiophene and phenyl rings on adjacent molecules with a distance between centroids of 3.79(2) ?. 相似文献18.
Crystallography Reports - Formation of the title Schiff base compound (E)-1-(((3-nitrophenyl)imino)methyl)naphthalen-2-ol, C17H12N2O3 (1) was achieved by the condensation of... 相似文献
19.
Crystallography Reports - A new six-coordinated Cd(II) polymer {[CdL2(H2O)2]?(H2O)}n (1) (HL = N-nicotinoylglycine) was synthesized with N-nicotinoylglycine, Cd(NO3)2?4H2O, NaOH and... 相似文献
20.
Khajuria Rajni Sharma Suresh Kapoor Kamal K. Gupta Vivek K. 《Crystallography Reports》2017,62(7):1144-1147
Crystallography Reports - The title compound 6-phenyl-4-(p-tolyl)pyridin-2(1H)-one was synthesized via one-pot, three component reaction of (E)-1-phenyl-3-(p-tolyl)-2-propen-1-one, ethyl... 相似文献