Effect of surface orientation on pool boiling heat transfer of nanoparticle suspensions

Several investigators have found that there is a significant effect of surface orientation on pool boiling performance and mechanisms, when a pure liquid is boiled over tubular heating surfaces. However, there is no similar study reported in literature for pool boiling of nanoparticle suspensions. This paper investigates the effect nanoparticles, suspended in pure liquids, can have on nucleate pool boiling heat transfer at various surface orientations. Systematic experiments were conducted on a smooth tube (average surface roughness 48 nm) of diameter 33 mm and length 170 mm at various inclinations (0°, 45° and 90°). Electro-statically stabilized water-based nanoparticle suspensions containing alumina nanoparticles (primary average sizes 47 nm and 150 nm) of concentrations 0.25%, 1% and 2% percent by weight were used. It has been found that there is a significant effect of surface orientation on the heat transfer performance. Horizontal orientation gave maximum heat transfer and the heating surface, when inclined at 45°, gave minimum heat transfer. Further, it was observed that surface–particle interaction and modified bubble motion can explain the behavior.     

Experimental study of critical heat flux enhancement during forced convective flow boiling of nanofluid on a short heated surface

Enhancements of nucleate boiling critical heat flux (CHF) using nanofluids in a pool boiling are well-known. Considering importance of flow boiling heat transfer in various practical applications, an experimental study on CHF enhancements of nanofluids under convective flow conditions was performed. A rectangular flow channel with 10-mm width and 5-mm height was used. A 10 mm-diameter disk-type copper surface, heated by conduction heat transfer, was placed at the bottom surface of the flow channel as a test heater. Aqueous nanofluids with alumina nanoparticles at the concentration of 0.01% by volume were investigated. The experimental results showed that the nanofluid flow boiling CHF was distinctly enhanced under the forced convective flow conditions compared to that in pure water. Subsequent to the boiling experiments, the heater surfaces were examined with scanning electron microscope and by measuring contact angle. The surface characterization results suggested that the flow boiling CHF enhancement in nanofluids is mostly caused by the nanoparticles deposition of the heater surface during vigorous boiling of nanofluids and the subsequent wettability enhancements.     

Influence of the aspect ratio on boiling flows in rectangular mini-channels

This article presents experiments conducted with two single rectangular mini-channels of same hydraulic diameter (1.4 mm) and different aspect ratios for conditions of horizontal boiling flow. The Forane® 365 HX used was subcooled (ΔT_sub = 15 °C) for all the boiling curves presented in the paper. Local heat transfer coefficients were measured for heat flux ranging from 25 to 62 kW m⁻² and mass flux from 200 kg m⁻² s⁻¹ to 400 kg m⁻² s⁻¹. The boiling flows were observed with two different cameras (depending on the flow velocity) through a visualization window. The flow patterns in the two channels were compared for similar conditions. The results show that the boiling heat transfer coefficient and the pressure drop values are different for the two single mini-channels. For low heat flux condition, the channel with lowest aspect ratio (H/W = 0.143) has a higher heat transfer coefficient. On the other hand, for high heat flux condition, the opposite situation occurs, namely the heat transfer coefficient becomes higher for the channel with highest aspect ratio (H/W = 0.43). This is probably due to the earlier onset of dryout in the channel with lowest aspect ratio. For the two cases of heating, the pressure drop for the two-phase flow remains lower for the channel with lowest aspect ratio. These results show that the aspect ratio plays a substantial role for boiling flows in rectangular channels. As for single-phase flows, the heat transfer characteristics are significantly influenced (even though the hydraulic diameter remains the same) by this parameter.     

Role of interfacial layer and clustering on the effective thermal conductivity of CuO-gear oil nanofluids

Copper oxide nanoparticles (∼40 nm) are dispersed in gear oil (IBP Haulic-68) at different volume fractions (0.005-0.025) with oleic acid added as a surfactant to stabilize the system. Prepared nanofluids are characterized by Fourier Transform Infrared spectroscopy (FTIR) and Dynamic light scattering (DLS) measurements. DLS data confirmed the presence of agglomerated nanoparticles in the prepared nanofluids. Thermal conductivity measurements are performed both as a function of CuO volume fraction and temperature between 5 and 80 °C. An enhancement in thermal conductivity at 30 °C of 10.4% with 0.025 volume fraction of CuO nanoparticle loading is observed. Measured volume fraction dependence of the thermal conductivity enhancement at room temperature is predicted fairly well considering contributions from both nanolayer at the solid-liquid interface and particle agglomeration in the suspension, as visualized by Feng et al.     

Experimental study of the characteristics and mechanism of pool boiling CHF enhancement using nanofluids

The pool boiling critical heat flux (CHF) performance of aqueous nanofluids was investigated using various nanoparticles of TiO₂, Al₂O₃, and SiO₂. The usage of a nanofluid as a working fluid can significantly enhance the pool boiling CHF, which was found to be strongly dependent on the kind of nanoparticle, as well as its concentration. A nanoparticle surface coating was observed on the heating surface after the experiment. The CHF of pure water on the nanoparticle-coated surface was higher than that of nanofluids for all cases. This revealed that the cause of the CHF enhancement using nanofluids is due to the fact that the heater surface is modified by the nanoparticle deposition. The mechanism of CHF enhancement due to the nanoparticle coating was discussed, relating it to surface wettability, surface roughness, and maximum capillary wicking height of the nanoparticle-coated surface.     

Subcooled flow boiling of R-134a in vertical channels of small diameter

Subcooled flow boiling heat transfer for refrigerant R-134a in vertical cylindrical tubes with 0.83, 1.22 and 1.70 mm internal diameter was experimentally investigated. The effects of the heat flux, q″ = 1–26 kW/m², mass flux, G = 300–700 kg/m² s, inlet subcooling, ΔT_sub,i = 5–15 °C, system pressure, P = 7.70–10.17 bar, and channel diameter, D, on the subcooled boiling heat transfer were explored in detail. The results are presented in the form of boiling curves and heat transfer coefficients. The boiling curves evidenced the existence of hysteresis when increasing the heat flux until the onset of nucleate boiling, ONB. The wall superheat at ONB was found to be essentially higher than that predicted with correlations for larger tubes. An increase of the mass flux leads, for early subcooled boiling, to an increase in the heat transfer coefficient. However, for fully developed subcooled boiling, increases of the mass flux only result in a slight improvement of the heat transfer. Higher inlet subcooling, higher system pressure and smaller channel diameter lead to better boiling heat transfer. Experimental heat transfer coefficients are compared to predictions from classical correlations available in the literature. None of them predicts the experimental data for all tested conditions.     

Visualization study of the effects of nanoparticles surface deposition on convective flow boiling CHF from a short heated wall

Enhancements of nucleate boiling critical heat flux (CHF) using nanofluids in a pool boiling are well known. Considering importance of flow boiling heat transfer in various practical applications, an experimental study on CHF enhancements of nanofluids under convective flow conditions was performed. Changing flow velocity from 0 m/s to 4 m/s, the water boiling on nanoparticles-coated heater was conducted and CHF increased at a given velocity. To understand clearly the mechanism of flow boiling CHF enhancement in nanofluid, the visualization of the nucleate boiling and CHF phenomenon was conducted using the high-speed video camera. It was found that the boiling heat transfer on the nanoparticles-coated heater was lower than that on bare heater, which induced the different flow regime at same heat flux. The different wetting zone on bare and nanoparticles-coated heaters was observed by visualization study. Based the wetting zone fraction, there was brief that the nucleate boiling fraction on heater would be related with the surface wettability. A new concept of flow boiling model was proposed based on the wetting zone fraction. Finally, the effect of nanoparticles deposition layer on the heater was interpreted with the physical mechanisms to increase CHF.     

Influence of nanoparticle surface coating on pool boiling

The purpose of this work is to study the effects of nanostructured surface coatings on boiling heat transfer and CHF. Boiling experiments are performed on a 100 μm diameter platinum wire immersed in saturated water or pentane at 1 bar. Nanostructured surface coating is obtained by deposition of charged γ-Fe₂O₃ nanoparticles (average diameter of 10 nm) on the platinum wire. Two different processes are compared: vigorous boiling and electrophoresis.The deposition of nanoparticles onto the heated surface induces a significant increase of the boiling critical heat flux (CHF) related to the increase of wettability. It also induces a decrease of the heat transfer coefficient when the wire is entirely covered with nanoparticles. The critical heat flux enhancement depends on the wettability of the fluid compared with the bare heater. Different physical mechanisms are also studied to explain the evolution of the characteristic parameters of the boiling on nanostructured surfaces.     

Boiling characteristics in small vertical tubes with closed bottom for nanofluids and nanoparticle-suspensions

An experimental study was carried out to understand the nucleate boiling characteristics and the critical heat flux (CHF) of water, the water based nanofluids and the water based nanoparticle-suspensions in vertical small heated tubes with a closed bottom. Here, the nanofluids consisted of the base liquid, the CuO nanoparticles and the surfactant. The nanoparticle-suspensions consisted of the base liquid and CuO nanoparticles. The surfactant was sodium dodecyl benzene sulfate. The study focused on the influence of the nanoparticles and surfactant on the nucleate boiling characteristics and the CHF. The experimental results indicated that the nanoparticle concentrations of the nanofluids and nanoparticle-suspensions in the tubes do not change during the boiling processes; the nanoparticles in the evaporated liquid are totally carried away by the steam. The boiling heat transfer rates of nanofluids are poorer than that of the base liquid. However, the boiling heat transfer rates of nanoparticle-suspensions are better than that of the base liquid. Comparing with the base liquid, the CHF of the nanofluids and the nanoparticle-suspensions is higher. The CHF is only related to nanoparticle mass concentration when the tube length and the tube diameter are fixed. The experiment confirm that there is a thin nanoparticle coating layer on the heated surface after the nanofluids boiling test but there is no coating layer on the heated surface after the nanoparticle-suspensions boiling test. This coating layer is the main reason that deteriorates the boiling heat transfer rates of nanofluids. An empirical correlation was proposed for predicting the CHF of nanofluids boiling in the vertical tubes with closed bottom.     

Experimental investigation of heat conduction in polyester-Al2O3 and polyester-CuO nanocomposites

This paper presents an experimental analysis of the thermal conductivity of nanocomposite systems composed of unsaturated polyester resin (UPR) as matrices and two different metal-oxides nanoparticles as fillers: alumina (aluminum oxide) and tenorite (copper oxide). The nanoparticles used were alpha-Al₂O₃ (30-40 nm) and CuO (30-50 nm). Samples were fabricated using simple molding and homogenization using magnetic stirring. Thermal conductivities were measured using a device that complies with ASTM norms C518-04 and E1530-06. Measurements were taken at three different temperatures (0 °C, 25 °C and 50 °C), for different sets of samples, varying the nanoparticle fraction used in composite systems. Finally, the experimental data are compared with traditional models for predicting the thermal conductivity of composite materials, showing that the traditional models underestimate the measured values.     

Pool boiling heat transfer performance of Newtonian nanofluids

Experimental measurements were carried out on the boiling heat transfer characteristics of γ-Al₂O₃/water and SnO₂/water Newtonian nanofluids. Nanofluids are liquid suspensions containing nanoparticles with sizes smaller than 100 nm. In this research, suspensions with different concentrations of γ-Al₂O₃ and SnO₂ nanoparticles in water were studied under nucleate pool boiling heat transfer conditions. Results show that nanofluids possess noticeably higher boiling heat transfer coefficients than the base fluid. The boiling heat transfer coefficients depend on the type and concentration of nanoparticles.     

Effect of surfactant additives on nucleate pool boiling heat transfer of refrigerant-based nanofluid

Effect of surfactant additives on nucleate pool boiling heat transfer of refrigerant-based nanofluid was investigated experimentally. Three types of surfactants including Sodium Dodecyl Sulfate (SDS), Cetyltrimethyl Ammonium Bromide (CTAB) and Sorbitan Monooleate (Span-80) were used in the experiments. The refrigerant-based nanofluid was formed from Cu nanoparticles and refrigerant R113. The test surface is horizontal with the average roughness of 1.6 μm. Test conditions include a saturation pressure of 101.3 kPa, heat fluxes from 10 to 80 kW m⁻², surfactant concentrations from 0 to 5000 ppm (parts per million by weight), and nanoparticle concentrations from 0 to 1.0 wt.%. The experimental results indicate that the presence of surfactant enhances the nucleate pool boiling heat transfer of refrigerant-based nanofluid on most conditions, but deteriorates the nucleate pool boiling heat transfer at high surfactant concentrations. The ratio of nucleate pool boiling heat transfer coefficient of refrigerant-based nanofluid with surfactant to that without surfactant (defined as surfactant enhancement ratio, SER) are in the ranges of 1.12-1.67, 0.94-1.39, and 0.85-1.29 for SDS, CTAB and Span-80, respectively, and the values of SER are in the order of SDS > CTAB > Span-80, which is opposite to the order of surfactant density values. The SER increases with the increase of surfactant concentration and then decreases, presenting the maximum values at 2000, 500 and 1000 ppm for SDS, CTAB and Span-80, respectively. At a fixed surfactant concentration, the SER increases with the decrease of nanoparticle concentration. A nucleate pool boiling heat transfer correlation for refrigerant-based nanofluid with surfactant is proposed, and it agrees with 92% of the experimental data within a deviation of ±25%.     

Enhanced nucleate boiling on copper micro-porous surfaces

Saturation boiling of PF-5060 dielectric liquid on Cu micro-porous surface layers (95, 139, 171, 197 and 220-μm thick) is investigated. These layers are deposited on 10 × 10 mm Cu substrates using two-stage electrochemical process. The basic micro-structure, obtained in the first stage using current density of 3 A/cm² for 15–44 s, depending on thickness, is strengthened by continuing electrochemical deposition using much lower current density for 10’s of minutes. For conditioned surface layers, after a few successive boiling tests, the pool boiling curves are reproducible and the temperature excursion prior to boiling incipience is either eliminated or reduced <7 K. Present nucleate boiling results are markedly better than those reported for dielectric liquids on micro- and macro-structured surfaces. Present values of CHF (22.7–27.8 W/cm²) and h_MNB (2.05–13.5 W/cm² K) are ∼40–70% higher than and >17 times those reported on plane surfaces (<16 W/cm² and ∼0.8 W/cm² K). Best results are those of the 171-μm thick layer: CHF of 27.8 W/cm² occurs at ΔT_sat of only 2.1 K and h_MNB of 13.5 W/cm² K occurs at ΔT_sat = 2.0 K.     

Nucleate boiling heat transfer in aqueous solutions with carbon nanotubes up to critical heat fluxes

In this study, pool boiling heat transfer coefficients (HTCs) and critical heat fluxes (CHFs) are measured on a smooth square flat copper heater in a pool of pure water with and without carbon nanotubes (CNTs) dispersed at 60 °C. Tested aqueous nanofluids are prepared using multi-walled CNTs whose volume concentrations are 0.0001%, 0.001%, 0.01%, and 0.05%. For the dispersion of CNTs, polyvinyl pyrrolidone polymer is used in distilled water. Pool boiling HTCs are taken from 10 kW/m² to critical heat flux for all tested fluids. Test results show that the pool boiling HTCs of the aqueous solutions with CNTs are lower than those of pure water in the entire nucleate boiling regime. On the other hand, critical heat flux of the aqueous solution is enhanced greatly showing up to 200% increase at the CNT concentration of 0.001% as compared to that of pure water. This is related to the change in surface characteristics by the deposition of CNTs. This deposition makes a thin CNT layer on the surface and the active nucleation sites of the surface are decreased due to this layer. The thin CNT layer acts as the thermal resistance and also decreases the bubble generation rate resulting in a decrease in pool boiling HTCs. The same layer, however, decreases the contact angle on the test surface and extends the nucleate boiling regime to very high heat fluxes and reduces the formation of large vapor canopy at near CHF. Thus, a significant increase in CHF results in.     

Boiling heat transfer characteristics of nanofluids in a flat heat pipe evaporator with micro-grooved heating surface

An experimental study was performed to understand the nucleate boiling heat transfer of water–CuO nanoparticles suspension (nanofluids) at different operating pressures and different nanoparticle mass concentrations. The experimental apparatus is a miniature flat heat pipe (MFHP) with micro-grooved heat transfer surface of its evaporator. The experimental results indicate that the operating pressure has great influence on the nucleate boiling characteristics in the MFHP evaporator. The heat transfer coefficient and the critical heat flux (CHF) of nanofluids increase greatly with decreasing pressure as compared with those of water. The heat transfer coefficient and the CHF of nanofluids can increase about 25% and 50%, respectively, at atmospheric pressure whereas about 100% and 150%, respectively, at the pressure of 7.4 kPa. Nanoparticle mass concentration also has significant influence on the boiling heat transfer and the CHF of nanofluids. The heat transfer coefficient and the CHF increase slowly with the increase of the nanoparticle mass concentration at low concentration conditions. However, when the nanoparticle mass concentration is over 1.0 wt%, the CHF enhancement is close to a constant number and the heat transfer coefficient deteriorates. There exists an optimum mass concentration for nanofluids which corresponds to the maximum heat transfer enhancement and this optimum mass concentration is 1.0 wt% at all test pressures. The experiment confirmed that the boiling heat transfer characteristics of the MFHP evaporator can evidently be strengthened by using water/CuO nanofluids.     

Carbon dioxide flow boiling in a single microchannel - Part II: Heat transfer

Flow boiling heat transfer coefficients of CO₂ have been measured in a single microchannel. Experiments were carried out in a horizontal stainless steel tube of 0.529 mm inner diameter, for three temperatures (−10, −5 and 0 °C), with the mass flux ranging from 200 to 1200 kg/m² s and the heat flux varying from 10 to 30 kW/m². The investigation covered qualities from zero to the dryout inception, i.e. pre-dryout conditions. Compared to larger microchannels and positive temperatures, a higher contribution of convective boiling was found, with a larger heat transfer coefficient than for pure nucleate boiling. Mainly two heat transfer regimes were found, depending on the boiling number (Bo). For Bo > 1.1 × 10⁻⁴, the heat transfer coefficient was highly dependent on the heat flux and moderately influenced by the quality and the mass flux. For Bo < 1.1 × 10⁻⁴, the heat transfer coefficient was hardly affected by the heat flux but strongly influenced by the quality and the mass flux. In addition, dryout results were reported. The effect of the mass flux on the dryout inception quality was found to be highly dependent on the heat flux and the saturation temperature.     

Series solutions for steady three-dimensional stagnation point flow of a nanofluid past a circular cylinder with sinusoidal radius variation

This article deals with the study of the steady three-dimensional stagnation point flow of a nanofluid past a circular cylinder that has a sinusoidal radius variation. By means of similarity transformation, the governing partial differential equations are reduced into highly non-linear ordinary differential equations. The resulting non-linear system has been solved analytically using an efficient technique namely homotopy analysis method (HAM). Expressions for velocity and temperature fields are developed in series form. In this study, three different types of nanoparticles are considered, namely alumina (Al₂O₃), titania (TiO₂), and copper (Cu) with water as the base fluid. For alumina–water nanofluid, graphical results are presented to describe the influence of the nanoparticle volume fraction φ and the ratio of the gradient of velocities c on the velocity and temperature fields. Moreover, the features of the flow and heat transfer characteristics are analyzed and discussed for foregoing nanofluids. It is found that the skin friction coefficient and the heat transfer rate at the surface are highest for copper–water nanofluid compared to the alumina–water and titania–water nanofluids.     

Boiling heat transfer characteristics of nanofluids jet impingement on a plate surface

The jet boiling heat transfer of a bar water–CuO particle suspensions (nanofluids) jet impingement on a large flat surface was experimentally investigated. The experimental results were compared with those from water. The quantificational effects of the nanoparticles concentration and the flow conditions on the nucleate boiling heat transfer and the critical heat flux (CHF) were investigated. The experimental data showed that the jet boiling heat transfer for the water–CuO nanofluid is significantly different from those for water. The nanofluids have poor nucleate boiling heat transfer compared with the base fluid due to that a very thin nanoparticle sorption layer was formed on the heated surface. The CHF for the nanofluid increased compared with that of water. The reasons were that the solid–liquid contact angle decreased due to a very thin sorption layer on the heated surface and the jet and agitating effect of the nanoparticles on the subfilm layer enhance supply of liquid to the surface.     

Viscosity of alumina nanoparticles dispersed in car engine coolant

The present paper, describes our experimental results on the viscosity of the nanofluid prepared by dispersing alumina nanoparticles (<50 nm) in commercial car coolant. The nanofluid prepared with calculated amount of oleic acid (surfactant) was tested to be stable for more than 80 days. The viscosity of the nanofluids is measured both as a function of alumina volume fraction and temperature between 10 and 50 °C. While the pure base fluid display Newtonian behavior over the measured temperature, it transforms to a non-Newtonian fluid with addition of a small amount of alumina nanoparticles. Our results show that viscosity of the nanofluid increases with increasing nanoparticle concentration and decreases with increase in temperature. Most of the frequently used classical models severely under predict the measured viscosity. Volume fraction dependence of the nanofluid viscosity, however, is predicted fairly well on the basis of a recently reported theoretical model for nanofluids that takes into account the effect of Brownian motion of nanoparticles in the nanofluid. The temperature dependence of the viscosity of engine coolant based alumina nanofluids obeys the empirical correlation of the type: log (μ_nf) = A exp(BT), proposed earlier by Namburu et al.     

Nucleate boiling and critical heat flux of HFE-7100 in horizontal narrow spaces

The pool boiling heat transfer and critical heat flux CHF of saturated HFE-7100 at atmospheric pressure on a confined smooth copper surface were experimentally studied. The horizontal upward boiling surface was confined by a face-to-face parallel unheated surface. We analysed the effects obtained by changing the diameter of the unheated surface and the gap between the boiling surface and the adiabatic surface. The gap values investigated were s = 0.5, 1.0, 2.0, 3.5 mm. To confine the circular boiling surface (d = 30 mm), two different Plexiglas discs were used: one with a diameter D = 30 mm, equal to that of the copper boiling surface, and the other with a diameter D = 60 mm, equal to that of the overall test section support. For each configuration, boiling curves were obtained up to the thermal crisis. For both configurations, it was observed that, at low wall superheat, the effect of confinement was not significant if Bo > 1, while for Bo ? 1 the heat transfer coefficient increased as the channel width s decreased. By contrast, at high wall superheat, a drastic reduction in both heat transfer and CHF was seen when the channel width s decreased; this reduction was less pronounced when the smaller confinement disc (D = 30 mm) was used. CHF data were also compared with the values predicted by literature correlations.