Ultrasonic imaging using air-coupled P(VDF/TrFE) transducers at 2 MHz

A reflection non-contact ultrasonic microscope system working both in amplitude and phase difference modes at 2 MHz has been developed using an air-coupled concave transducer made of piezoelectric polymer films of poly(vinylidene fluoride/trifluoroethylene) [P(VDF/TrFE)]. The transducer is composed of three 95 μm-thick P(VDF/TrFE) films stacked together, each of which is activated electrically in parallel by a driving source. The transducer has a wide aperture angle of 140° and a focal length of 10 mm. The measured two-way transducer insertion loss is 80 dB at 1.83 MHz. Despite 20 dB higher insertion loss than that estimated from Mason’s equivalent circuit, we have obtained clear amplitude acoustic images of a coin with transverse resolution of 150 μm, and clear phase difference acoustic images of the rough surface of a paper currency bill with depth resolution of sub-micrometer. Using two planar transducers of P(VDF/TrFE), we have also successfully measured in through-transmission mode the sound velocity and absorption of a 3 mm-thick silicone-rubber plate. The present study proves that, owing to its low acoustic impedance and flexibility, P(VDF/TrFE) piezoelectric film is very useful for high frequency acoustic imaging in air in the MHz range.     

Wavelength tunable,high energy femtosecond laser pulses directly generated from large-mode-area photonic crystal fiber

Wavelength tunable high energy ultrashort laser pulses are generated from a large-mode-area photonic crystal fiber in anomalous dispersion (AD) regime. A simplified laser cavity design with one fine polished facet of the fiber as a cavity mirror is used. The intra-cavity dispersion compensation is achieved by a grating pair, the spatial dispersed light from which also have optical spectrum filtering effects combined with the limited aperture of the fiber core. The laser system is able to generate ultrashort pulses ranging from 494 fs (with 56 nJ pulse energy) to 1.24 ps (with 49 nJ pulse energy) at 55 MHz repetition rate. The filtering mechanism benefits the generation of high energy pulses with narrowing pulse duration in AD regime. An undulation in frequency and time domain is also observed with the increase of the pump power. Furthermore, this laser system is directly used as seed for supercontinuum generation.     

Nanosecond-pulsed erbium-doped fiber lasers with graphene saturable absorber

We demonstrate graphene mode-locked nanosecond erbium-doped fiber laser in an all-fiber ring cavity. The clean and robust pulse train was generated at 27 mW pump power. Resultant central wavelength, repetition rate and pulse width was 1560 nm, 388 kHz and 6 ns, respectively. With two stage fiber amplifier, the output power was 553 mW, corresponding to single pulse energy of 1.4 μJ. In addition, the pulse-width can be varied ranging from 3 ns to 20 ns at repetition rate between 200 kHz and 1.54 MHz by changing the length of the laser cavity.     

Generation of long bursts of high-repetition-rate arbitrarily shaped optical pulses using time lens

A technique for the generation of long ultrahigh-speed bursts of optical pulses with arbitrary shapes is proposed. A laser pulse is temporally chirped by a time lens and then passes through a filter with a reconfigurable periodic spectral response, which produces time-delayed replicas of the chirped pulse and recombines them. As a result of the temporal interference between the replicas, the chirped pulse is broken up into short pulses with the shape determined by the chosen filter response. It is demonstrated that the filter acts on a long chirped optical pulse as a temporal modulator with a periodic modulation function. The modulation frequency and bandwidth of the modulator can be much higher than for commercially available high-frequency modulators. The additional advantage of this modulator is the arbitrary shape of the modulation function. A 2.4 ns burst of nearly flat-top pulses with a repetition rate of about 400 GHz is obtained in numerical simulations. In addition, the technique proposed can act as a pulse repetition rate multiplier and a pulse compressor. A repetition rate of 1.589 THz and an individual pulse width of 212 fs are achieved in simulations for a 9.7 ns sinusoidally phase modulated pulse burst.     

Investigation of Q-switched InP-based 1550 nm semiconductor lasers

High energy picosecond pulse generation from a two contact tapered 5 quantum well (QW) InGaAlAs/InP diode laser (1550 nm) is investigated using a passive Q-switching technique. Single peak pulses with pulse energies as high as 500 pJ and durations of typically hundreds of picoseconds are obtained from the device by applying reverse bias voltages in the range of 0 V to ?18 V to the absorber section of the device. It is also demonstrated that more symmetrical Q-switched pulses are obtained by reducing the duration of electrical pulses applied to the gain section of the laser. Such an improvement is attributed to the reduced time of the population inversion in the gain section due to shorter electrical pulse. We also show comparatively the dependence of optical spectra on the reverse bias voltage for diode lasers emitting at 1550 nm and 1350 nm, and demonstrate that better spectral output is obtained from AlGaInAs lasers emitting at a wavelength of 1550 nm.     

2 μm passive Q-switched mode-locked Tm3+:YAP laser with single-walled carbon nanotube absorber

We report the first demonstration, to our knowledge, of passive Q-switched mode-locking in a Tm³⁺:YAP laser, operating in the 2 μm broadly spectral region formed with a compact Z-flod cavity. A transmission-type single-walled carbon nanotube saturable absorber (SWCNT–SA) is used for the initiation of the pulse generation. The repetition rate of the Q-switched envelope was 60 kHz at the pump power of 8.6 W. The mode-locked pulses inside the Q-switched pulse envelope had a repetition rate of ～92 MHz. A maximum average output power of 761 mW was obtained. The dependence of the operational parameters on the pump power was also investigated experimentally.     

Wide-band fanned-out supercontinuum source covering O-, E-, S-, C-, L- and U-bands

A wide-band supercontinuum source generated by mode-locked pulses injected into a Highly Non-Linear Fiber (HNLF) is proposed and demonstrated. A 49 cm long Bismuth–Erbium Doped Fiber (Bi–EDF) pumped by two 1480 nm laser diodes acts as the active gain medium for a ring fiber laser, from which mode-locked pulses are obtained using the Non-Polarization Rotation (NPR) technique. The mode-locked pulses are then injected into a 100 m long HLNF with a dispersion of 0.15 ps/nm km at 1550 nm to generate a supercontinuum spectrum spanning from 1340 nm to more than 1680 nm with a pulse width of 0.08 ps and an average power of ?17 dBm. The supercontinuum spectrum is sliced using a 24 channel Arrayed Waveguide Grating (AWG) with a channel spacing of 100 GHz to obtain a fanned-out laser output covering the O-, E-, S-, C-, L- and U-bands. The lasing wavelengths obtained have an average pulse width of 9 ps with only minor fluctuations and a mode-locked repetition rate of 40 MHz, and is sufficiently stable to be used in a variety of sensing and communication applications, most notably as cost-effective sources for Fiber-to-the-Home (FTTH) networks.     

Creaming enhancement in a liter scale ultrasonic reactor at selected transducer configurations and frequencies

Recent research has shown that high frequency ultrasound (0.4–3 MHz), can enhance milkfat separation in small scale systems able to treat only a few milliliters of sample. In this work, the effect of ultrasonic standing waves on milkfat creaming was studied in a 6 L reactor and the influence of different frequencies and transducer configurations in direct contact with the fluid was investigated. A recombined coarse milk emulsion with fat globules stained with oil-red-O dye was selected for the separation trials. Runs were performed with one or two transducers placed in vertical (parallel or perpendicular) and horizontal positions (at the reactor base) at 0.4, 1 and/or 2 MHz (specific energy 8.5 ± 0.6 kJ/kg per transducer). Creaming behavior was assessed by measuring the thickness of the separated cream layer. Other methods supporting this assessment included the measurement of fat content, backscattering, particle size distribution, and microscopy of samples taken at the bottom and top of the reactor. Most efficient creaming was found after treatment at 0.4 MHz in single and double vertical transducer configurations. Among these configurations, a higher separation rate was obtained when sonicating at 0.4 MHz in a vertical perpendicular double transducer setup. The horizontal transducer configuration promoted creaming at 2 MHz only. Fat globule size increase was observed when creaming occurred. This research highlights the potential for enhanced separation of milkfat in larger scale systems from selected transducer configurations in contact with a dairy emulsion, or emulsion splitting in general.     

Design and construction of Q-switched Nd:YAG laser system for LIBS measurements

A passive, Q-switched pulsed, Nd:YAG laser system was designed and built, which can provide a potential compact robust laser source for portable laser induced breakdown spectroscopy systems.The developed laser system operates at 1064 nm. Each laser shot contains a train of pulses having maximum total output energy of 170 mJ. The number of pulses varies from 1–6 pulses in each laser shot depending on the pump energy. The pulse width of each pulse ranges from 20 to 30 ns. The total duration of the output pulse train is within 300 μs. The multi-pulse nature of the laser shots was employed to enhance the LIBS signal. To validate the system, LIBS measurements and analysis were performed on ancient ceramic samples collected from Al-Fustat excavation in Old Cairo. The samples belong to different Islamic periods in Egypt history. The results obtained are highly indicative that useful information can be provided to archeologists for use in restoring and repairing of precious archeological objects.     

Ultrasound pressure distributions generated by high frequency transducers in large reactors

The performance of an ultrasound reactor chamber relies on the sound pressure level achieved throughout the system. The active volume of a high frequency ultrasound chamber can be determined by the sound pressure penetration and distribution provided by the transducers. This work evaluated the sound pressure levels and uniformity achieved in water by selected commercial scale high frequency plate transducers without and with reflector plates. Sound pressure produced by ultrasonic plate transducers vertically operating at frequencies of 400 kHz (120 W) and 2 MHz (128 W) was characterized with hydrophones in a 2 m long chamber and their effective operating distance across the chamber’s vertical cross section was determined. The 2 MHz transducer produced the highest pressure amplitude near the transducer surface, with a sharp decline of approximately 40% of the sound pressure occurring in the range between 55 and 155 mm from the transducer. The placement of a reflector plate 500 mm from the surface of the transducer was shown to improve the sound pressure uniformity of 2 MHz ultrasound. Ultrasound at 400 kHz was found to penetrate the fluid up to 2 m without significant losses. Furthermore, 400 kHz ultrasound generated a more uniform sound pressure distribution regardless of the presence or absence of a reflector plate. The choice of the transducer distance to the opposite reactor wall therefore depends on the transducer plate frequency selected. Based on pressure measurements in water, large scale 400 kHz reactor designs can consider larger transducer distance to opposite wall and larger active cross-section, and therefore can reach higher volumes than when using 2 MHz transducer plates.     

Fundamental and harmonic mode-locking in erbium-doped fiber laser based on graphene saturable absorber

Graphene-based passively mode-locked erbium doped fiber laser is presented. Multilayer graphene was obtained by mechanical exfoliation of pure graphitic block and deposited on the fiber ferrule. The mode-locking performance was investigated under various laser pumping conditions. The laser could operate at fundamental repetition rate of 16.34 MHz with 844 fs pulse duration and 30 mW average output power. Also harmonic-mode locking of the laser is demonstrated. 294 and 800 MHz repetition rates were obtained (corresponding to the 18th and 49th harmonic of the fundamental repetition frequency, respectively) with nearly transform-limited pulses.     

10 GHz ultra-stable short optical pulse generation via phase-modulation enhanced dual-loop optoelectronic oscillator

We report on a high rate, ultra-low timing jitter, short optical pulse generator based on cascaded amplitude and phase modulation in an optoelectronic oscillator. The radio-frequency supermodes are shown to be greatly suppressed with the dual-loop architecture, and a highly coherent and flat optical frequency comb is generated. Optical pulses of 12.8 ps duration are obtained with 27.5 fs integrated timing jitter from 100 Hz to 10 MHz.     

Distributed fiber sensing system with wide frequency response and accurate location

A distributed fiber sensing system merging Mach–Zehnder interferometer and phase-sensitive optical time domain reflectometer (Φ-OTDR) is demonstrated for vibration measurement, which requires wide frequency response and accurate location. Two narrow line-width lasers with delicately different wavelengths are used to constitute the interferometer and reflectometer respectively. A narrow band Fiber Bragg Grating is responsible for separating the two wavelengths. In addition, heterodyne detection is applied to maintain the signal to noise rate of the locating signal. Experiment results show that the novel system has a wide frequency from 1 Hz to 50 MHz, limited by the sample frequency of data acquisition card, and a spatial resolution of 20 m, according to 200 ns pulse width, along 2.5 km fiber link.     

Using of sonochemically prepared SbSI for electrospun nanofibers

A novel polymeric, polyacrylonitrile (PAN) nanofibers containing ferroelectric and semiconducting antimony sulfoiodide (SbSI) have been made by electrospinning. SbSI nanowires, used as the filler, have been prepared sonochemically from antimony sulphide (Sb₂S₃) and antimony tri-iodide (SbI₃) for the first time. Nanocrystalline SbSI has been fabricated in ethanol under ultrasonic irradiation (20 kHz, 565 W/cm²) at 323 K within 2 h. The products have been characterized by using techniques such as powder X-ray diffraction, scanning electron microscopy, energy dispersive X-ray analysis, high-resolution transmission electron microscopy, selected area electron diffraction and optical diffuse reflection as well as transmission spectroscopy. The good quality of the nanocrystals and their dispersion in the nanofiber’s volume is important because this material is attractive for nanogenerators due to its ferroelectric and piezoelectric properties. The amplitude of the voltage pulse, generated under shock pressure of 3.0 MPa, has reached 180 V in the prototype PAN/SbSI piezoelectric nanogenerator. The peak output voltage of about 0.2 V was measured in bending/releasing conditions with the deformation frequency of 1 Hz.     

Electrical characterization of dielectric barrier discharge driven by repetitive nanosecond pulses in atmospheric air

Dielectric barrier discharge (DBD) is an important method to produce non-thermal plasma, which has been widely used in many fields. In the paper, a repetitive nanosecond-pulse generator is used for the excitation of DBD. Output positive pulse of the generator has a rise time of about 15 ns and a full width at half maximum of 30–40 ns, and pulse repetition frequency varies from single shot to 2 kHz. The purpose of this paper is to experiment the electrical characteristics of DBD driven by repetitive nanosecond pulses. The variables affecting discharge conditions, including air gap spacing, dielectric thickness, barrier fashion, and applied pulse repetition frequency, are investigated. The relationship between electric field, discharge current, instantaneous discharge power across air gap, and estimated electron density with the length of air gap, dielectric thickness, barrier fashion, and pulse repetition frequency is obtained respectively, and the experimental results are also discussed. In addition, two typical images exhibiting homogeneous and filamentary discharges are given with different experimental conditions.     

Optical delay with spectral hole burning in Doppler-broadened cesium vapor

The full frequency dependence of the optical delay in the Cs D₁ (6 ²S_1/2 ? 6 ²P_1/2) line has been observed, including all four hyperfine split components. Pulse delays of 1.6 ns to 24.1 ns are obtained by scanning across the hyperfine splitting associated with the lower ²S_1/2 state. Optical control of pulse delays in cesium vapor was demonstrated by pumping the D₂ (6 ²S_1/2 ? 6 ²P_3/2) transition and observing resulting holes in the D₁ delay spectrum. For a pump at four times the saturation intensity, the pulse delays are reduced by a maximum of 78% in a narrow region of 110 MHz. The frequency dependence of the delays of the probe laser in the vicinity of the spectral holes agrees with a Kramers–Kronig model prediction.     

Degradation of nitrobenzene in aqueous solution by dual-pulse ultrasound enhanced electrochemical process

The present work reports a novel dual-pulse ultrasound enhanced electrochemical degradation (US-ECD) process that synchronizes alternatively ultrasound pulses and potential pulses to degrade nitrobenzene in aqueous solution with a high percentage degradation and low energy consumption. In comparison to the test results generated from the conventional US-ECD and original electrochemical degradation (ECD) process, the dual-pulse US-ECD process increased degradation percentages to nitrobenzene by 2% and 17%, respectively, while energy used in the pulse process was only about 46.5% of that was used in the conventional US-ECD process. Test results demonstrated a superior performance of the dual-pulse US-ECD process over those of other conventional ones. Impacts of pulse mode, initial pH value, cell voltage, supporting electrolyte concentration and ultrasonic power on the process performances were investigated. With operation conditions optimized in the study at pH = 3.0, cell voltage = 10 V, ultrasonic power = 48.84 W, electrolyte concentration = 0.1 M and an experiment running time of 30 min, the percentage degradation of nitrobenzene could reach 80% (US pulse time = 50 ms and ECD pulse time = 50 ms). This process provided a reliable and effective technical approach to degrade nitrobenzene in aqueous solution and significantly reduced energy consumption in comparison to the conventional US-ECD or original ECD treatment.     

Precise spatial control of cavitation erosion in a vessel phantom by using an ultrasonic standing wave

In atherosclerotic inducement in animal models, the conventionally used balloon injury is invasive, produces excessive vessel injuries at unpredictable locations and is inconvenient in arterioles. Fortunately, cavitation erosion, which plays an important role in therapeutic ultrasound in blood vessels, has the potential to induce atherosclerosis noninvasively at predictable sites. In this study, precise spatial control of cavitation erosion for superficial lesions in a vessel phantom was realised by using an ultrasonic standing wave (USW) with the participation of cavitation nuclei and medium-intensity ultrasound pulses. The superficial vessel erosions were restricted between adjacent pressure nodes, which were 0.87 mm apart in the USW field of 1 MHz. The erosion positions could be shifted along the vessel by nodal modulation under a submillimetre-scale accuracy without moving the ultrasound transducers. Moreover, the cavitation erosion of the proximal or distal wall could be determined by the types of cavitation nuclei and their corresponding cavitation pulses, i.e., phase-change microbubbles with cavitation pulses of 5 MHz and SonoVue microbubbles with cavitation pulses of 1 MHz. Effects of acoustic parameters of the cavitation pulses on the cavitation erosions were investigated. The flow conditions in the experiments were considered and discussed. Compared to only using travelling waves, the proposed method in this paper improves the controllability of the cavitation erosion and reduces the erosion depth, providing a more suitable approach for vessel endothelial injury while avoiding haemorrhage.     

Diode-pumped Nd:YAG ceramic laser at 946 nm passively Q-switched with a Cr4+:YAG saturable absorber

We demonstrate a diode-pumped Nd:YAG ceramic laser with emission at 946 nm that is passively Q-switched by single-crystal Cr⁴⁺:YAG saturable absorber. An average output power of 1.7 W is measured under 18.4 W of incident power using an output mirror with transmission T=4%. The corresponding optical-to-optical efficiency is 9.2%. The laser runs at a pulse repetition rate of 120 kHz and delivers pulses with energy of 14 μJ and duration of 80 ns, which corresponds to a peak power of 175 W.     

All fiber passively mode locked zirconium-based erbium-doped fiber laser

All passively mode locked erbium-doped fiber laser with a zirconium host is demonstrated. The fiber laser utilizes the Non-Linear Polarization Rotation (NPR) technique with an inexpensive fiber-based Polarization Beam Splitter (PBS) as the mode-locking element. A 2 m crystalline Zirconia–Yttria–Alumino-silicate fiber doped with erbium ions (Zr–Y–Al-EDF) acts as the gain medium and generates an Amplified Spontaneous Emission (ASE) spectrum from 1500 nm to 1650 nm. The generated mode-locked pulses have a spectrum ranging from 1548 nm to more than 1605 nm, as well as a 3-dB bandwidth of 12 nm. The mode-locked pulse train has an average output power level of 17 mW with a calculated peak power of 1.24 kW and energy per pulse of approximately 730 pJ. The spectrum also exhibits a Signal-to-Noise Ratio (SNR) of 50 dB as well as a repetition rate of 23.2 MHz. The system is very stable and shows little power fluctuation, in addition to being repeatable.