Laser welding of glasses using a nanosecond pulsed Nd:YAG laser

This work reports on laser welding of two 1 mm thickness borosilicate glasses through the irradiation with a nanosecond pulsed laser, as a novel alternative to the use of ultrashort pulsed lasers for welding of transparent materials. Two different methodologies were investigated and compared in terms of interface quality. In a first approach, the glasses were joined without any absorbing intermediate layer. However, the bond interface possesses defects. To improve the resulting bond interface, the use of a titanium ultrathin intermediate layer was proposed to weld the glasses substrates, acting as a sealant between them. The laser parameters were optimized to achieve the best joining conditions of the Ti film. The use of the Ti layer gives rise to a bond interface more homogeneous and free of damages. As a further step, thin glasses of 86 µm thickness, of great technological value, were joined through the Ti film as well. The joined interfaces were inspected through optical microscopy and scanning electron microscopy (SEM) while the bond quality was evaluated by Scanning Acoustic Microscopy (SAM).     

Spectroscopic characterization of low-nickel copper welding with pulsed Nd:YAG laser

Effects of various operating parameters of 400 W pulsed Nd:YAG laser on welding of nickel-alloyed copper have been investigated. The induced plume spectra in case of using different assist gases and preheat temperatures have been analyzed and the effects of these key factors on melt features such as penetration depth, porosity and spattering have been attributed to the spectroscopic behavior of the plume. Moreover, the CuI electron temperature and its standard deviation as the spectroscopic responses of the plasma plume to various laser process parameters have been quantitatively evaluated at different average and peak powers and pulse energies. Also, the mentioned responses were utilized to justify the weld bead profile features, involving weld depth, width and their stabilities, at similar process parameters. The operating conditions of welding were optimized, regarding the results of spectroscopic observations and attributing them to the qualitative aspects of the melt pool.     

Biocompatible film deposition by using Nd:YAG pulsed laser

A Nd:YAG laser operating at the fundamental wavelength (1064 nm) and at the second harmonic (532 nm), with 9 ns pulse duration, 100–900 mJ pulse energy, and 30 Hz repetition rate mode, was employed to ablate in vacuum (10^?6 mbar) biomaterial targets and to deposit thin films on substrate backings. Titanium target was ablated at the fundamental frequency and deposited on near-Si substrates. The ablation yield increases with the laser fluence and at 40 J/cm ² the ablation yield for titanium is 1.2×10¹⁶ atoms/pulse. Thin film of titanium was deposited on silicon substrates placed at different distance and angles with respect to the target and analysed with different surface techniques (optical microscopy, scanning electron spectrosopy (SEM), and surface profile).

Hydroxyapatite (HA) target was ablated to the second harmonic and thin films were deposited on Ti and Si substrates. The ablation yield at a laser fluence of 10 J/cm ² is about 5×10¹⁴ HA molecules/pulse. Thin film of HA, deposited on silicon substrates placed at different distance and angles with respect to the target, was analysed with different surface techniques (optical microscopy, SEM, and Raman spectroscopy).

Metallic films show high uniformity and absence of grains, whereas the bio-ceramic film shows a large grain size distribution. Both films found special application in the field of biomaterial coverage.     

Stable seeder-injected Nd:YAG pulsed laser using a RbTiOPO_4 phase modulator

A stable, single-longitudinal-mode, nanosecond-pulsed Nd:YAG laser with a laser-diode dual-end pumping arrangement is constructed. Injection seeding is performed successfully by utilizing a Rb Ti OPO4 crystal as the intracavity phase modulator to change the optical length of the slave cavity based on the delay-ramp-fire technique. The laser generates 9.9 m J of pulse energy with a 16 ns pulse duration at a 400 Hz repetition rate.A near-diffraction-limit laser beam is achieved with a beam quality factor M2 of approximately 1.2. The frequency jitter is 1.5 MHz over 2 min, and the fluctuation of the output pulse power is 0.3% over 23 min.     

UV laser micromachining of piezoelectric ceramic using a pulsed Nd:YAG laser

UV laser (=355 nm) ablation of piezoelectric lead zirconate titanate (PZT) ceramics in air has been investigated under different laser parameters. It has been found that there is a critical pulse number (N=750). When the pulse number is smaller than the critical value, the ablation rate decreases with increasing pulse number. Beyond the critical value, the ablation rate becomes constant. The ablation rate and concentrations of O, Zr and Ti on the ablated surface increase with the laser fluence, while the Pb concentration decreases due to the selective evaporation of PbO. The loss of the Pb results in the formation of a metastable pyrochlore phase. ZrO₂ was detected by XPS in the ablated zone. Also, the concentrations of the pyrochlore phase and ZrO₂ increase with increasing laser fluence. These results clearly indicate that the chemical composition and phase structure in the ablated zone strongly depend on the laser fluence. The piezoelectric properties of the cut PZT ceramic samples completely disappear due to the loss of the Pb and the existence of the pyrochlore phase. After these samples were annealed at 1150 °C for 1 h in a PbO-controlled atmosphere, their phase structure and piezoelectric properties were recovered again. Finally, 1–3 and concentric-ring 2–2 PZT/epoxy composites were fabricated by UV laser micromachining and their thickness modes were measured by impedance spectrum analysis and a d₃₃ meter. Both composites show high piezoelectric properties. PACS 81.40.Gh; 77.84.-s     

Investigation of Cr:YAG passive mode-locking in a pulsed Nd:YAG laser

Passive mode-locking of a pulsed Nd:YAG laser using a Cr⁴⁺:YAG saturable absorber was realized for the first time in a nearly critical stable resonator containing an antiresonant ring structure. The output energy and pulse duration are 13.5 mJ and 180 ps, respectively. The recovery time and saturable intensity for excited-state absorption of Cr⁴⁺:YAG under the action of strong laser pulses were calculated from rate equations.     

A keyhole volumetric model for weld pool analysis in Nd:YAG pulsed laser welding

This study presents a new model for analyzing the temperature distribution and weld pool shape in Nd:YAG pulsed laser welding. In the proposed approach, a surface flux heat transfer model is applied in the low laser energy intensity region of the weld, while a keyhole heat transfer model based on a volumetric heat source is applied in the high laser energy intensity region of the weld. The correlation between the intensity of the laser input energy and the geometric parameters of the volumetric heat source is derived experimentally. A series of MARC finite element simulations based on the proposed single pulse model are performed to investigate the shape and size of the weld pool given different laser energy intensities. A good agreement is observed between the simulation results and the experimental results obtained under equivalent single pulse welding conditions. Thus, the basic validity of the proposed model is confirmed.     

Quality of the beam produced a pulsed Nd:YAG laser

The quality of the beam produced by a Nd:YAG laser was investigated. A hemispherical Nd:YAG laser resonator was developed. A flashlamp driver was designed to pump a Nd:YAG laser crystal. The output of the laser was characterized via the variation of the capacitor voltage. A phosphor card was used to detect the invisible of the infrared beam. Exposed photographic paper was utilized to examine the energetic beam after interaction. The brightness and strength of the beams were analyzed using the Matrox Inspector and VideoTest 5 software packages. The intensity of the beam produced and the volume loss after interaction were found to linearly increase with respect to the input energy.     

Experimental study of electro-optical-switched pulsed Nd:YAG laser

We report the specification of a compact and stable side diode-pumped Q-switched pulsed Nd:YAG laser. We experimentally study and compare the performance of the pulsed Nd:YAG laser in the free-running and Q-switched modes at different pulse repetition rates from 1 Hz to 100 Hz. The laser output energy is stabilized by using a special configuration of the optical resonator. In this laser, an unsymmetrical concave–concave resonator is used and this structure helps the mode volume to be nearly fixed when the pulse repetition rate is increased. According to the experimental results in the Q-switched operation, the laser output energy is nearly constant around 70 m J with an FWHM pulse width of 7 ns at100 Hz. The optical-to-optical conversion efficiency in the Q-switched regime is 17.5%.     

Gas protection optimization during Nd:YAG laser welding

Many laser processes, such as welding or surface treatments are associated with an undesired phenomenon, which is oxidation. The solution commonly employed to solve this problem approaches the shielding gas and/or the shielding gas device. What we propose in this paper is a methodology with the goal to optimize the protection gas device design as well as the gas flow in the case of laser welding and surface treatments. The pressure created by the gas flow on the sample surface is recorded and analysed together with the operating parameters influence in order to reach the objectives. The nozzle system designed and presented below assures the protection against material oxidation using minimal gas flow rates and increases the welding penetration in the case of high-power Nd:YAG laser welding.     

In-process vibration-assisted high power Nd:YAG pulsed laser ceramic–metal composite cladding on Al-alloys

An in-process vibration-assisted laser cladding method was designed for improving the shrinkage cavities of pulsed Nd:YAG laser ceramic–metal composite cladding on Al-alloys. The substrate was vibrated during the cladding process. A signal generator in this study externally modulated the frequency, amplitude, and wave shape of the vibration. An acceleration sensing device was used to monitor the vibration condition to ensure the modulation was correct. The feasibility of using the in-process vibration-assisted method for improving the shrinkage cavities of pulsed Nd:YAG laser SiC+Al–Si cladding on an Al-alloy was then experimentally evaluated. The experimental results show that the in-process vibration-assisted method significantly improves the degree of cavity shrinkage when the penetration depth is not very great. Analysis of the data shows that with vibration-assisted cladding, the depth of penetration increases with frequencies between 200 and 1500 Hz. The results were especially significant for 800 mV modulation vibration.     

Hollow-fiber delivery of high-power pulsed Nd:YAG laser light

We propose hollow fibers for delivery of high-peak-power pulsed Nd:YAG laser light. Hollow fibers with an internal polymer layer were fabricated by a liquid-phase coating technique. We reduced the losses of the fibers in the near-infrared region by producing a silver film that was very smooth owing to use of an ultrasonic wave for mixing of the silver and the reducer solutions in the silver-plating process. The straight losses of the 1-m-long polymer-coated fibers were 0.3 dB for the 700-mum bore size and 0.1 dB for the 1000-mum bore fiber.     

高功率高光束质量脉冲Nd: YAG激光器

以实现高功率、高光束质量的脉冲激光输出为目的,对非对称平-凹谐振腔的结构进行了理论分析。设计出了高功率、高光束质量非对称放置的平-凹谐振腔、双氙灯泵浦的脉冲Nd: YAG激光器。当占空比为9%时,实现输出激光平均功率近480 W,光束参数积优于12.7 mm·mrad,电光转化效率近4%,与理论分析吻合,可用芯径300 μm的光纤传输,不稳定性优于±1%。加工实验证明有较好的质量：切割材料为不锈钢,厚度为3 mm时、切割速度为0.6 m/min和厚度为1.5 mm、切割速度为1.2 m/min时,两种情况下所得切缝宽度均为250 μm,且切割上下沿光滑。     

Experimental study of electro-optical Q-switched pulsed Nd:YAG laser

We report the specification of a compact and stable side diode-pumped Q-switched pulsed Nd:YAG laser. We experimentally study and compare the performance of the pulsed Nd:YAG laser in the free-running and Q-switched modes at different pulse repetition rates from 1 Hz to 100 Hz. The laser output energy is stabilized by using a special configuration of the optical resonator. In this laser, an unsymmetrical concave-concave resonator is used and this structure helps the mode volume to be nearly fixed when the pulse repetition rate is increased. According to the experimental results in the Q-switched operation, the laser output energy is nearly constant around 70 mJ with an FWHM pulse width of 7 ns at 100 Hz. The optical-to-optical conversion efficiency in the Q-switched regime is 17.5%.     

高功率高光束质量脉冲Nd: YAG激光器

 以实现高功率、高光束质量的脉冲激光输出为目的,对非对称平-凹谐振腔的结构进行了理论分析。设计出了高功率、高光束质量非对称放置的平-凹谐振腔、双氙灯泵浦的脉冲Nd: YAG激光器。当占空比为9%时,实现输出激光平均功率近480 W,光束参数积优于12.7 mm·mrad,电光转化效率近4%,与理论分析吻合,可用芯径300 μm的光纤传输,不稳定性优于±1%。加工实验证明有较好的质量：切割材料为不锈钢,厚度为3 mm时、切割速度为0.6 m/min和厚度为1.5 mm、切割速度为1.2 m/min时,两种情况下所得切缝宽度均为250 μm,且切割上下沿光滑。     

Enhanced drilling using a dual-pulse Nd:YAG laser

A new method for improving the efficiency of laser drilling has been developed. Two synchronized free-running laser pulses from a tandem-head Nd:YAG laser are capable of drilling through 1/8-in-thick stainless-steel targets at a stand-off distance of 1 m without gas-assist. The combination of a high-energy laser pulse for melting with a properly tailored high-intensity laser pulse for liquid expulsion results in the efficient drilling of metal targets. We argue that the improvement in drilling is due to the recoil pressure generated by rapid evaporation of the molten material by the second laser pulse. Received: 29 August 2000 / Accepted: 18 December 2000 / Published online: 3 April 2001     

Simple optical apparatus for trepanning and percussion microdrilling using pulsed green Nd:YAG laser

Laser microdrilling is becoming an important tool in a wide spectrum of industrial applications due to the possibility to produce microholes in almost any type of materials. The purpose of this study was to create a simple and efficient optical apparatus that could produce microdrillings by either percussion or trepanning methods. The developed system is composed by a nanosecond Nd:YAG laser operating at 532 nm and one convergent lens with off-center optical axis of 1′. For the trepanning method the lens spins in its geometrical center at constant angular speed of 350 rpm. Typical microholes diameters obtained in metallic aluminum were in the range of 22 to 95 μm and 70 to 150 μm for the percussion and trepanning methods, respectively. Typical drilling velocities were in the order of 10 μm/s for applied fluences ranging from 22 to 150 J/cm² for both methods. The values of the ratio between input and output diameters were 0.30 and 0.25 for microholes obtained by percussion and trepanning methods, respectively. The best microholes morphology was obtained using the trepanning method. The results for both methods are discussed based on the optical and thermal properties of the material processed and the constructed apparatus.     

Thin films of silver nanoparticles deposited in vacuum by pulsed laser ablation using a YAG:Nd laser

We report the deposition of thin films of silver (Ag) nanoparticles by pulsed laser ablation in vacuum using the third line (355 nm) of a YAG:Nd laser. The nanostructure and/or morphology of the films was investigated as a function of the number of ablation pulses, by means of transmission electron microscopy and atomic force microscopy. Our results show that films deposited with a small number of ablation pulses (500 or less), are not continuous, but formed of isolated nearly spherical Ag nanoparticles with diameters in the range from 1 nm to 8 nm. The effect of increasing the number of pulses by one order of magnitude (5000) is to increase the mean diameter of the globular nanoparticles and also the Ag areal density. Further increase of the number of pulses, up to 10,000, produces the formation of larger and anisotropic nanoparticles, and for 15,000 pulses, quasi-percolated Ag films are obtained. The presence of Ag nanoparticles in the films was also evidenced from the appearance of a strong optical absorption band associated with surface plasmon resonance. This band was widened and its peak shifted from 425 nm to 700 nm as the number of laser pulses was increased from 500 to 15,000.     

用倍频晶体KTP实现Nd：YAG激光锁模的研究

报道用倍频晶体KTP实现Nd:YAG激光锁模的系统研究,给出了该锁模激光器输出脉宽的表达式,并和实验测量值相比较,计算值跟实验结果符合较好.文中还分析了各种参数对该锁模激光输出性能的影响.