Scholte波与含泥沙两相流介质属性关系的分析及仿真验证

基于四种超声悬浮液模型Urick, Urick-Ament, HT, Mcclements分析了Scholte波在两相流体与多孔介质固体界面处的传播特性. 结合各模型的复波数表达式建立含泥沙流体-多孔介质固体界面波特征方程, 分析了Scholte波速与两相流体积含量、粒径等介质属性的关系. 通过仿真实验获得界面波信号, 运用时延估计获得Scholte波速与泥沙含量、粒径的关系, 发现所得的波速与Urick-Ament和HT理论有相对好的一致性. 关键词： Scholte波 两相流体 多孔介质 泥沙含量     

Ultrasonic velocity in water-ethanol-sucrose mixtures during alcoholic fermentation

During alcoholic fermentation, sucrose and water are transformed into ethanol and carbon dioxide by the action of yeast enzymes. The measurement of the velocity of an ultrasonic pulse travelling through a fermentation tank can be used to characterize the state of the process. In this work, an experimental study of the density and ultrasonic velocity in the ternary mixture (water-ethanol-saccharose) is presented. Experimental results were compared to ideal density and to commonly used expressions of the sound velocity in liquid mixtures (Urick, Natta-Baccaredda and Nomoto). A semiempirical approach was proposed to improve the efficiency of theoretical models when dealing with mixtures of associated liquids.     

Laser ultrasound characterization of chemically prepared nano-structured silver

The ultrasonic properties of nano-structured silver (hereafter nm-Ag) are investigated by the laser ultrasonic technique. The nm-Ag superfine particles with a size of 20 to 27 nanometer (nm) are prepared by using a chemical method. Wafers of nm-Ag are fabricated under different pressing pressures and used as samples. The experimental results show that the ultrasonic velocity and attenuation of nm-Ag prepared by the chemical method depends on the pressing pressures and thus on the relative density. The elastic moduli values of nm-Ag prepared by the chemical method are deduced. The values are lower than those of polycrystalline and single-crystalline Ag. The detailed results, discussions, and comparisons with nm-Ag samples prepared by a physical method are presented. Received: 23 November 1998 / Accepted: 13 September 1999 / Published online: 24 March 2000     

Extraction of silver from a refractory silver ore by sono-cyanidation

In this study, effect of ultrasound on silver extraction from a refractory silver ore containing both native silver and various silver sulphide minerals was investigated. Main effects and interaction effects of pulp density, ultrasonic frequency, cyanide concentration, air flow rate and agitation speed on the extraction rate of silver were studied by a two-level fractional factorial experimental design. A few additional cyanidation tests were also conducted to verify the findings of the designed experiments.It was found that the overall extraction yield was varied from 67% to 90% depending on the operating conditions used in the sono-cyanidation tests (48 h). However, it was varied from 63% to 80% by same operating conditions used in the direct cyanidation tests at the same cyanidation time. It was observed that an increase in the ultrasonic frequency has a negligible effect on the silver recovery. More importantly, it was determined that there were insignificant differences between the 24-h sono-cyanidation results and the 48-h direct cyanidation results for each cyanidation conditions. This finding, which is very important from the cyanidation practice standpoint, indicates that the cyanidation time can be reduced up to 50%, or the capacity of an operating silver extraction plant can be increased up to 100% by the sono-cyanidation by the refractory silver ores. In order to describe the rate of silver dissolution in the cyanide solutions, the experimental data were analysed using shrinking core models. It was found that there is a good fit between the experimental data and the models, indicating the rate of silver dissolution in cyanide can be described by a two-stage, porous layer diffusion controlled, shrinking core model.     

A probability density function of liftoff velocities in mixed-size wind sand flux

With the discrete element method (DEM), employing the diameter distribution of natural sands sampled from the Tengger Desert, a mixed-size sand bed was produced and the particle-bed collision was simulated in the mixed-size wind sand movement. In the simulation, the shear wind velocity, particle diameter, incident velocity and incident angle of the impact sand particle were given the same values as the experimental results. After the particle-bed collision, we collected all the initial velocities of rising sand particles, including the liftoff angular velocities, liftoff linear velocities and their horizontal and vertical components. By the statistical analysis on the velocity sample for each velocity component, its probability density functions were obtained, and they are the functions of the shear wind velocity. The liftoff velocities and their horizontal and vertical components are distributed as an exponential density function, while the angular velocities are distributed as a normal density function. Supported by the Key Project of the National Natural Science Foundation of China (Grant No. 10532040)     

Use of a silver ion selective electrode to assess mechanisms responsible for biological effects of silver nanoparticles

For a detailed analysis of the biological effects of silver nanoparticles, discrimination between effects related to the nano-scale size of the particles and effects of released silver ions is required. Silver ions are either present in the initial particle dispersion or released by the nanoparticles over time. The aim of this study is to monitor the free silver ion activity {Ag⁺} in the presence of silver nanoparticles using a silver ion selective electrode. Therefore, silver in the form of silver nanoparticles, 4.2 ± 1.4 nm and 2–30 nm in size, or silver nitrate was added to cell culture media in the absence or presence of A549 cells as a model for human type II alveolar epithelial cells. The free silver ion activity measured after the addition of silver nanoparticles was determined by the initial ionic silver content. The p {Ag⁺} values indicated that the cell culture media decrease the free silver ion activity due to binding of silver ions by constituents of the media. In the presence of A549 cells, the free silver ion activity was further reduced. The morphology of A549 cells, cultivated in DME medium containing 9.1% (v/v) FBS, was affected by adding AgNO₃ at concentrations of ≥30 μM after 24 h. In comparison, silver nanoparticles up to a concentration of 200 μM Ag did not affect cellular morphology. Our experiments indicate that the effect of silver nanoparticles is mainly mediated by silver ions. An effect of silver on cellular morphology was observed at p {Ag⁺} ≤ 9.2.     

银颗粒表面尿嘧啶分子的SERS实验研究——KCl对尿嘧啶分子吸附状态的影响

利用表面增强喇曼散射(SERS)在灰银胶体系中研究了KCl对尿嘧啶分子吸附状态的影响,并将实验结果与Oh等人在黄银胶体系中的实验结果进行了详细比较.对这一实验现象进行了定性解释.     

CFD-DEM simulation of three-dimensional aeolian sand movement

A three-dimensional CFD-DEM model is proposed to investigate the aeolian sand movement.The results show that the mean particle horizontal velocity can be expressed by a power function of heights.The probability distribution of the impact and lift-off velocities of particles can be described by a log-normal function,and that of the impact and lift-off angles can be expressed by an exponential function.The probability distribution of particle horizontal velocity at different heights can be described as a lognormal function,while the probability distribution of longitudinal and vertical velocity can be described as a normal function.The comparison with previous two-dimensional calculations shows that the variations of mean particle horizontal velocity along the heights in two-dimensional and three-dimensional models are similar.However,the mean particle density of the two-dimensional model is larger than that in reality,which will result in the overestimation of sand transportation rate in the two-dimensional calculation.The study also shows that the predicted probability distributions of particle velocities are in good agreement with the experimental results.     

Estimating organic chain length through sound velocity measurements

The ability to measure the length of polymers while monitoring their production is evidently extremely valuable, but is also a useful tool for chemical identification purposes at other times, e.g. the analysis of waste water. A study of the relationship between velocity of sound and chain length has been carried out. Initial studies were performed on two model systems; a series of pure liquid n-alkanes (pentane to hexadecane) and 1-alcohols (methanol to 1-dodecanol). This study was extended to look at an industrially significant system of dimethylsiloxanes 200 fluid (L2, 0.65 cSt) to 200 fluid (5000 cSt). Corresponding density data have been taken from the literature and the adiabatic compressibility determined. The measured adiabatic compressibility has been compared with two molecular models of wound velocity, the Schaaffs model and a development of the Urick equation. The Urick equation approach is based on a determination of the compressibility of the methylene or siloxane repeat units which make up the chains in these linear molecules. We show that the Urick equation approach accurately predicts sound velocity and compressibility for the higher members of each series, whilst the Schaaffs approach fails for the 1-alcohols. We suggest that this is because of the influence of the hydroxyl end group through hydrogen bonding with methylene groups within the chain. This interaction modifies the derived compressibility of the methylene groups, so reducing their compressibility relative to that of the n-alkanes. The technique described provides valuable new insights into end-group, intermolecular and intra-molecular interactions in liquid linear-chain molecules. From this detailed analysis of the mechanisms involved, a model is derived. This model can give very precise estimations of the composition of a pure liquid. In the case of mixtures of polymers, it is necessary to use the modified Urick equation and then, in addition, the concentration dependence of both the velocity of sound and the density must be measured.     

Ultrasonic determination of the particle size distribution in water-based magnetic liquid

Magnetic liquids are stable colloidal suspensions of nano-sized magnetic particles in a carrier liquid medium. In the present paper the determination of the particle size distribution function using ultrasonic spectroscopy is described. The ultrasonic spectra of water-based magnetic fluid measured in the 3.5-50 MHz frequency range are analyzed using formulas for the velocity and absorption of sound in dispersion media obtained by Vinogradov. The results of the ultrasonic studies are compared with the particles size distribution function evaluated from the processing of the magnetic susceptibility data.     

The KdV-Burgers equation in speed gradient viscous continuum model

Based on the microscopic two velocity difference model, a macroscopic model called speed viscous continuum model is developed to describe traffic flow. The relative velocities are added to the motion equation, which leads to viscous effects in continuum model. The viscous continuum model overcomes the backward travel problem, which exists in many higher-order continuum models. Nonlinear analysis shows that the density fluctuation in traffic flow leads to density waves. Near the onset of instability, a small disturbance could lead to solitons described by the Korteweg-de Vries-Burgers (KdV-Burgers) equation, which is seldom found in other traffic flow models, and the soliton solution is derived.     

Ultrasonic wave propagation in heterogeneous solid media: theoretical analysis and experimental validation

This research deals with the ultrasonic characterization of thermal damage in concrete. This damage leads to the appearance of microcracks which then evolve in terms of volume rate and size in the material. The scattering of ultrasonic waves from the inclusions is present in this type of medium. The propagation of the longitudinal wave in the heterogeneous media is studied via a homogenization model that integrates the multiple scattering of waves. The model allows us to determine the phase velocity and the attenuation according to the elements which make the medium. Simulations adapted to the concrete are developed in order to test the responses of the model. These behaviors are validated by an experimental study: the measurements of phase velocity and attenuation are performed in immersion, with a comparison method, on a frequency domain which ranges from 160 kHz to 1.3 MHz. The analysis of different theoretical and experimental results obtained on cement-based media leads to the model validation, on the phase velocity behavior, in the case of a damage simulated by expanded polystyrene spheres in granular media. The application to the case of a thermally damaged concrete shows a good qualitative agreement for the changes in velocity and attenuation.     

Two sub-pixel processing algorithms for high accuracy particle centre estimation in low seeding density particle image velocimetry

This article presents two algorithms for spatial processing of low seeding density PIV (particle image velocimetry) images which lead to sub-pixel precision in particle positioning. The particle centres are estimated to accuracies of the order of 0.1 pixel, yielding 1% error in velocity calculation. The first algorithm discriminates valid particles from the rest of the image and determines their centres in Cartesian coordinates by using a two-dimensional Gaussian fit. The second algorithm performs local correlation between particle pairs and determines instantaneous two-dimensional velocities. The methods have been applied initially to simulated data. Gaussian noise and distortion has then been added to simulate experimental conditions. It is shown that, in comparison with conventional methods, the new algorithms offer up to an order of magnitude higher accuracy for particle centre estimation. Finally, the Gaussian fit approach has been used to map an experimental transonic flow field from the stator trailing edge wake region of a cascade with an estimated error of 1%. The experimental results are found to be in good agreement with previous theoretical steady-state viscous calculations.     

Nanoporous carbon spheres and their application in dispersing silver nanoparticles

Monodisperse nanoporous carbon spheres (NCS) were synthesized in large quantities via a facile hydrothermal synthesis. It is found that the NCS have rough surfaces with a large quantity of uniformly distributed protruding and concaving zones. Large quantities of nanopores of about 0.3 nm in diameter are distributed uniformly on the whole sphere surfaces. The effects of reaction parameters on the surface roughness, sphere diameter and pore size of NCS were investigated. Taking the NCS as substrates, silver nanoparticles (NPs) were deposited onto their surfaces using a one-step ultrasonic electrodeposition procedure. The deposited silver NP has a uniform distribution, a high particle density and a narrow size range of 12-16 nm in diameter. This study demonstrates an efficient approach to fabricate noble-metal/carbon nanocomposites.     

Ultrasonic measurements of the two characteristic lengths in fibrous materials

In a method for measuring the two characteristic lengths in rigid frame porous media proposed by Leclaire et al. [Ph. Leclaire, L. Keiders, W. Lauriks. Determination of the viscous and thermal characteristic lengths of plastic foams by ultrasonic measurements in helium and air. J Appl Phys 1996;80:2009–12] ultrasonic transmission measurements are made through a sample of material when it is saturated with two different gases. It is shown that the accuracy of this method can be limited when the porous medium in saturated with helium as proposed originally. A considerable improvement in the signal-to-noise ratio can be achieved if argon is used instead of helium because the characteristic impedance is higher and the viscous skin depth in argon is 3 times less than that in helium. This paper also discusses the measurement of the tortuosity and the sound velocity in glass wool.     

On the gravitational motion of a nonuniformly heated solid particle in a gaseous medium

The steady motion of a nonuniformly heated spherical aerosol particle through a viscous gaseous medium is theoretically studied in the Stokes approximation. It is assumed that the mean temperature of the particle surface may differ appreciably from the ambient temperature. The solution of gasdynamic equations yields an analytical expression for the drag of the medium and the gravitational fall velocity of the nonuniformly heated spherical solid particle with allowance for the temperature dependence of the density of the medium and molecular transfer coefficients (viscosity and thermal conductivity). Numerical estimates show that heating of the particle surface considerably influences the drag force and gravitational fall velocity.     

Insulator-based dielectrophoresis in viscous media—Simulation of particle and droplet velocity

The velocity of micro-particles in a nonuniform electric field was examined as a function of electrical potential and particle size to illustrate the possible application of dielectrophoresis (DEP) as a new separation technique in viscous media. A new comprehensive model is presented that combines the effects of DEP and electrohydrodynamic forces on particle motion. The current model simulation takes into account the possible significant influence of electrohydrodynamic effects depending on the particle size, electrode distance, and voltage applied during DEP particle separation. The heat generated as a consequence of high electric field strength leads to density gradients in the liquid, thus inducing buoyancy forces that cause fluid convective motion.Experimental velocity measurements using two materials having extreme properties, i.e. polyethylene (PE) particles (diameter range 100–2000 μm) and water droplets (diameter range 25–275 μm), both suspended in a viscous medium (silicone oil), correspond with the proposed theoretical predictions. The comprehensive model presented was applied to insulator-based DEP in a direct current (dc) electric field, but it is expected to allow predictions of various similar systems.     

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用密度调制的方法研究了等离子体中粒子输运问题。采用了注入脉冲式补充送气和超声分子束两种不同的密度调制方法。在HL-2A装置常规欧姆放电的情况下,运用有限差分法和Nagashima矩阵技术,求解了粒子平衡方程。计算出了粒子的输运系数(对流速度v和扩散系数D)。研究了粒子输运系数与等离子体线平均密度之间的关系。实验结果表明,在欧姆放电的情况下,等离子体芯部的粒子对流速度方向始终是向内的,并且密度低时,粒子输运系数(粒子扩散系数D和对流速度v)较大;密度高时,粒子输运系数较小。     

The use of ultrasonic standing waves to enhance optical particle sizing equipment

Fluid dynamics modelling augmented with routines to simulate acoustic forces on aerosol particles has been used to investigate the potential of combining ultrasonic standing wave fields with optical particle analysis equipment. Simulations of particle dynamics in airstreams incorporating acoustic forces predict that particles in the 1-10 microns diameter range may be effectively focused to the velocity nodes of the standing wave field. Particles move to the velocity nodes within tens of milliseconds for acoustic frequencies of 10-100 kHz and at an acoustic energy density of 100 Jm-3. Larger particles are predicted to move to the velocity antinodes within similar times; however, there is a crossover region at approximately 15-20 microns particle diameter where longer times are predicted due to the competing forces driving particles to the vibration node and antinode. With sufficient transverse flow velocities the models predict that disturbances due to acoustic streaming can be overcome and a useful degree of focusing achieved for the aerosol particles. Results from a model demonstrating sampling and acoustic focusing of 3-9 microns aerosol particles to a 200 microns wide analysis area are presented.     

A study of nanosized zinc oxide and its nanofluid

The synthesis and characterization of nanosized zinc oxide and its nanofluid in a polyvinyl alcohol (PVA) matrix have been done in the present investigation. Crystalline zinc oxide nanoparticles are synthesized using single-step chemical method while the nanofluids are prepared by the dispersion of nanoparticles in PVA solution using an ultrasonicator. The prepared nanoparticles are characterized using X-ray diffraction, SEM?CEDX and UV?Cvisible spectrum. The particle size distribution measurement is carried out by acoustic particle sizer. The ultrasonic velocities are measured in the synthesized nanofluid under different physical conditions using an ultrasonic interferometer. It is found that the degree of crystallinity of nanoparticles depends on the evaporation rate during its synthesis and ultrasonic velocity has non-linear relation with temperature for the present nanofluid.