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银耳状BiOBr的制备及光催化性能研究
引用本文:曹丰璞,丁呈华,仲治国,柳文敏.银耳状BiOBr的制备及光催化性能研究[J].影像科学与光化学,2014,32(6):558-564.
作者姓名:曹丰璞  丁呈华  仲治国  柳文敏
作者单位:南阳师范学院 化学与制药工程学院, 河南 南阳 473061
基金项目:国家自然科学青年基金项目,河南省教育厅自然科学研究项目,南阳师范学院高层次人才科研启动费项目资助
摘    要:以β-环糊精(β-CD)、硝酸铋、溴化钾为原料,采用溶剂热法合成了银耳状BiOBr.通过X射线衍射(XRD)、扫描电镜(SEM)和紫外可见光谱(UV-Vis)对BiOBr粒子进行表征.实验发现:BiOBr的微观形貌与β-CD的用量有关,当β-CD的用量为0.4574 g时,所制得的BiOBr为银耳状,且其光催化性能最好.

关 键 词:&beta  -环糊精  溶剂热  银耳状BiOBr  光催化  
收稿时间:2014-04-25

Preparation of Tremella-like BiOBr and Its Photocatalytic Performance
CAO Fengpu,DING Chenghua,ZHONG Zhiguo,LIU Wenmin.Preparation of Tremella-like BiOBr and Its Photocatalytic Performance[J].Imaging Science and Photochemistry,2014,32(6):558-564.
Authors:CAO Fengpu  DING Chenghua  ZHONG Zhiguo  LIU Wenmin
Affiliation:College of Chemistry and Pharmaceutical Engineering, Nanyang Normal University, Nanyang 473061, Henan, P. R. China
Abstract:A solvothermal method to prepare tremella-like BiOBr was developed by using β-CD, Bi(NO3)3·5H2O and KBr as starting materials. The nano BiOBr was characterized by X-ray diffraction, scanning electron microscopy(SEM) and UV-visible. It was found that the micro-morphology of BiOBr was greatly influenced by the amount of β-CD. When the amount of β-CD was 0.4574 g, the morphology of product was tremella-like BiOBr with a highest photocatalytic activity under visible light irradiation.
Keywords:β-CD  solvothermal  tremella-like BiOBr  photocatalytic
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