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Synthesis of flower-like WS2 by chemical vapor deposition
Affiliation:1.Institute of Physics & Optoelectronics Technology, Baoji University of Arts and Sciences, Baoji 721016, China;2.School of Science, Xi'an University of Posts & Telecommunications, Xi'an 710121, China
Abstract:Flower-like tungsten disulfide (WS2) with a diameter of 5-10 μm is prepared by chemical vapor deposition (CVD). Scanning electron microscopy (SEM), energy dispersive spectrometer (EDS), Raman spectroscopy, and ultraviolet-visible (UV-vis) spectroscopy are used to characterize its morphological and optical properties, and its growth mechanism is discussed. The key factors for the formation of flower-like WS2 are determined. Firstly, the cooling process causes the generation of nucleation dislocations, and then the "leaf" growth of flower-like WS2 is achieved by increasing the temperature.
Keywords:flower-like WS2  chemical vapor deposition (CVD)  optical property  growth mechanism  
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