水热法合成掺杂铁离子的小管径TiO2纳米管
Preparation of Fe-doped TiO2 Nanotubes with Small Diameter by Hydrothermal Method
作者单位E-mail
宋旭春 浙江大学化学系, 杭州, 310027  
岳林海 浙江大学化学系, 杭州, 310027  
刘波 浙江大学化学系, 杭州, 310027  
韩贵 浙江大学化学系, 杭州, 310027  
陈卫祥 浙江大学化学系, 杭州, 310027  
徐铸德 浙江大学化学系, 杭州, 310027 chexzd@mail.hz.zj.cn 
摘要: 碳纳米管这种一维结构的新材料的发现为物理、化学、材料科学和纳米科学开辟了全新的研究领域.近年来,非碳无机类富勒烯(Inorganic Fullerenelike,简称IF)纳米管也受到人们的广泛关注.
关键词: 水热法  二氧化钛  掺杂  纳米管
基金项目: 国家自然科学基金资助项目(No.20171039;50171036);浙江省自然科学基金资助项目(No.200053)
Abstract: Using Fe-doped titania powders as the precursor, Fe-doped TiO2 nanotubes with small diameter of 10nm were obtained by hydrothermal method. The doped titania powders have two different crystalline phases, anatase and rutile of which the average particle diameters are 30.3nm and 41.7nm, receptively. The products were characterized by TEM, XRDand EDS. The results showed that Fe-doped TiO2 nanotubes of 200nm in length could be obtained from Fe-doped rutile powder, and have higher yields. The formation mechanism of long titania nanotubes was suggested in the light of the relative stability of crystalline phase.
Keywords: hydrothermal method  titania  doping  nanotube
投稿时间:2003-01-03 修订日期:2003-03-24
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宋旭春,岳林海,刘波,韩贵,陈卫祥,徐铸德.水热法合成掺杂铁离子的小管径TiO2纳米管[J].无机化学学报,2003,19(8):899-901.
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